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Sodium Picramate

Sodium chlorate Sodium nitrate Sodium perchlorate Sodium picramate... [Pg.35]

Sodium picramate Sodium 2-amino-4,6-dinitrophenolate, Sodium... [Pg.114]

DMSO, Sodium azide, DINA, Methylene chloride. Sodium sulfate. Activated alumina Methyl green. Sodium picramate. Hydrochloric acid. Sodium nitrate... [Pg.136]

Nitric acid. Kerosene, Ammonium picramate. Ethanol Sodium picramate. Hydrochloric acid. Sodium nitrate Nitric acid. Diethanolamine, Acetic anhydride. Acetyl chloride. Acetone, Potassium carbonate Acetic anhydride. Hydrochloric acid. Diethanolamine, Methylene chloride. Nitric acid. Sodium bicarbonate Nitric acid. Diethanolamine, Hydrogen chloride. Sodium bicarbonate Diisopropylamine, Nitric acid... [Pg.136]

Figure A. 151 Sodium picramate primary high explosive. Figure A. 151 Sodium picramate primary high explosive.
Sodium picramate, dry or wetted with less than 20 % water, by mass 1349... [Pg.121]

The sodium picramate starting material is itself explosive, but is commercially available as a chemical intermediate. It can be made by the reduction of picric acid with reducing agents such as sodium sulfide. The key to making useful DDNP is to control the rate of diazotization so that relatively large, rounded crystals are formed instead of needles or platelets that do not flow or pack well. [Pg.1756]

Summary Diazodinitrophenol can be prepared by reacting sodium picramate with nitrous acid. The nitrous acid is generated on-sight by the reaction between sodium nitrite and hydrochloric acid. The diazodinitrophenol precipitates when it forms, due to the excessive amount water present in the reaction mixture. The product is then easily filtered-off, washed, and then dried. Commercial Industrial note For related, or similar information, see Serial No. 181,028, December 21st, 1937, by Hercules Powder Company, to Leon W. Babcock, Kenvil, NJ. Part or parts of this laboratory process may be protected by international, and/or commcrcial/industrial processes. Before using this process to legally manufacture the mentioned explosive, with intent to sell, consult any protected commercial or industrial processes related to, similar to, or additional to, the process discussed in this procedure. This process may be used to legally prepare the mentioned explosive for laboratory, educational, or research purposes. [Pg.91]

Summary Diazodinitrophenol is prepared by reacting sodium picramate with sodium nitrite, and hydrochloric acid. Diazodinitrophenol is then precipitated in a special manner by the addition of a methyl green indicator. The methyl green... [Pg.93]

Hazards Note sodium picramate is also a high explosive. Wear gloves and use proper ventilation when handling 35% hydrochloric acid. 35% Hydrochloric acid is highly corrosive and toxic. [Pg.94]

LEAD-TNP, BARIUM STYPHANTE, LEAD STYPHNATE, AMMONIUM PICRAMATE, AMMONIUM PICRATE, LEAD PICRATE, SODIUM PICRAMATE... [Pg.302]

Sodium picramate. Ammonium 2-ami no-4,6-dinitrophenol ate Ammoni um-2-ami no-4,6-di nitropi crate... [Pg.313]

Sodium picramate forms stable crystals, which ignite rapidly and burn violently. The crystals are used in priming compositions for bullets and the like, initiation compositions for blasting caps and detonators, high performance rocket propellants, fireworks and a variety of pyrotechnics compositions for flares, incendiaries, and signals. It is also used as an intermediate in the production of other high explosives. Sodium picramate should be stored submerged in kerosene. ... [Pg.313]

See other pages where Sodium Picramate is mentioned: [Pg.513]    [Pg.7]    [Pg.14]    [Pg.349]    [Pg.129]    [Pg.129]    [Pg.180]    [Pg.180]    [Pg.286]    [Pg.242]    [Pg.1147]    [Pg.380]    [Pg.690]    [Pg.1755]    [Pg.1755]    [Pg.24]    [Pg.91]    [Pg.92]    [Pg.92]    [Pg.93]    [Pg.93]    [Pg.94]    [Pg.94]    [Pg.313]    [Pg.313]    [Pg.91]   
See also in sourсe #XX -- [ Pg.242 ]

See also in sourсe #XX -- [ Pg.242 ]

See also in sourсe #XX -- [ Pg.242 ]

See also in sourсe #XX -- [ Pg.242 ]

See also in sourсe #XX -- [ Pg.242 ]



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