Protocols determinations

Most experimental protocols determine the time of harvest from the application dates of the experimental chemical product. If the study s Principal Investigator has guessed correctly months earlier when the first application was made, the crop will be at the proper maturity when harvested. However, if the weather or some other factor changes, the crop may be immature or over-ripe. If the experimental protocol does not permit for these variations in growing conditions, there may be an adverse impact on the ability to process the test samples properly, possibly resulting in atypical processed fraction samples. [Pg.222]

The study protocol determines the quantities of raw materials to be processed. The protocol should state the quantity of each fraction sample to be provided and whether multiple samples are to be drawn from each fraction sample. The wording of the protocol should allow for a range of quantities that is to be provided for each processes commodity to avoid having to prepare protocol deviations. For example, stating that a minimum of 1 lb of pur6e is to be provided avoids a protocol deviation if the processor provides 1.1 lb of purde. [Pg.223]

Basic Protocol Determination of Water Activity in Food Samples by... [Pg.35]

Alternate Protocol Determination of Water Activity Corrected for Change in... [Pg.35]

Alternate Protocol Determination of Peptidase Activity Using a... [Pg.349]

Alternate Protocol Determination of Both Neutral and Polar Lipids by TLC-FID Dl.6.7... [Pg.423]

Alternate Protocol Determination of Peroxide Value by Measurement... [Pg.513]

ALTERNATE PROTOCOL DETERMINATION OF PEROXIDE VALUE BY MEASUREMENT OF IRON OXIDATION The ferrous oxidation/xylenol orange (FOX) method is based on the ability of lipid peroxides to oxidize ferrous ions at low pH. The resulting oxidation is quantitated by using a dye that complexes with the generated ferric ions to produce a color that can be measured spectrophotometrically. Peroxide values (PVs) as low as 0.1 meq active oxygen/kg sample can be determined with this method, providing a distinct advantage over iodometric titration. [Pg.520]

D3.1 Determination of Solid Fat Content by Nuclear Magnetic Resonance Basic Protocol Determining Solid Fat Content by a Direct Parallel NMR D3.1.1... [Pg.565]

Basic Protocol Determination of Reducing and Nonreducing Sugars Using the Phenol-Sulfuric Acid Assay... [Pg.651]

Alternate Protocol Determination of Noncellulosic Neutral Sugars and... [Pg.695]

Validation Protocol Determination of Compound X and its Related Compounds in Product X Tablets... [Pg.162]

Validation Protocol Determination of Trace Levels of Element A in Product B Tablets... [Pg.168]

Method-Transfer Protocol Determination of Substance J and Related Compounds in Tablets... [Pg.174]

The clinical protocol determines whether the protocol will expose subjects to unnecessary risks. The protocol contains the qualifications and credentials of the investigator(s). The protocols are very detailed including the qualifications of all professionals administering the nonapproved drug product. Protocols for each phase of clinical study are required. All human research subjects must be informed of all the risks and benefits of the drug product. Informed consent must be obtained from all subjects prior to enrollment in the clinical trial. [Pg.22]

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