Procedure 9.3 Infrared Spectroscopic Analysis of VO acac

Note pyridine is toxic, and must be used only in the hood. Avoid contact with your skin. [Pg.221]

Record the IR spectrum (KBr pellet) of the VO(acac)2 complex (see Procedure 3.4). [Pg.221]

Compare the spectrum of VO(acac)2 with that of 2,4-pentanedione, prepared neat with salt plates. [Pg.221]

Take solution IR spectra of VO(acac)2 in methylene chloride (CH2CI2), acetonitrile (CH3CN), and pyridine using 0.2 mm NaCl solution cells. [Pg.222]

Answer the questions and fill out the Results Summary sheet. [Pg.222]

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