Oils Refractive

The resolution of the instrument in the vertical direction depends upon the wavelength of visible light (450 to 850 nm), the oil refractive index, and the difference between the maximum and the minimum interference intensity as follows [5,18] ... 

To demonstrate that the gradient effect can be removed in an aligned system, similar experiments were performed by measuring a homogeneous sample of mineral oil (refractive index c 1.48), using both the ZnSe ATR accessory and the diamond ATR accessory (Supercritical Fluid Analyzer, Specac, UK). Both results... 

Production of oil. Colour of oil Refraction 15 C.. Optical rotation 15 C. Specific gravity 15 C.. ... 

Fat or oil Solidification point, °C Specific gravity (15°C/15°C) Refractive index Acid value Saponification value Iodine value... 

Tables 4 and 5 show properties of ground mica products. For all forms of ground mica the index of refraction is 1.58 wt %, Mohs hardness is 2.5, oil absorption (Brit. Stand. 3483) is 60.75%, water solubihty (Brit. Stand. 1765) is <0.3%, the phericity factor is 0.01, and the softening point in °C is 1538. For Microni2ed and wet ground micas the brightness (green filter), pH, and apparent density in kg/m are 75, 5.2, and 160—224, respectively for dry ground mica, 66—75, 6.2, and 192—561, respectively (1).

Refraction Index. Refraction index is deterrnined with a petrographic microscope by submersing a sample in emersion oils of known refractive index. 

Other terms relating to physical properties include viscosity refractive index pour point, ie, the lowest temperature at which the oil flows flash point, ie, the temperature at which the oil ignites and aniline point, ie, the minimum temperature at which equal volumes of oil and aniline are completely miscible. These are determined under defined conditions estabHshed by ASTM. 

Chemical modification of the wax can improve smear resistance (5). Sihcones, which do not harm furniture finishes (6), are incorporated as film-forming ingredients in furniture pohshes. The lubricant properties of sihcones improve ease of apphcation of the pohsh and removal of insoluble soil particles. In addition, sihcones make dry films easier to buff and more water-repeUent, and provide depth of gloss, ie, abihty to reflect a coherent image as a result of a high refractive index (7). Wax-free pohshes, which have sihcones as the only film former, can be formulated to dehver smear resistance (8). Another type of film former commonly used in oil-base furniture pohshes is a mineral or vegetable oil, eg, linseed oil. 

When simple Hquids like naphtha are cracked, it may be possible to determine the feed components by gas chromatography combined with mass spectrometry (gc/ms) (30). However, when gas oil is cracked, complete analysis of the feed may not be possible. Therefore, some simple definitions are used to characterize the feed. When available, paraffins, olefins, naphthenes, and aromatics (PONA) content serves as a key property. When PONA is not available, the Bureau of Mines Correlation Index (BMCI) is used. Other properties like specific gravity, ASTM distillation, viscosity, refractive index. Conradson Carbon, and Bromine Number are also used to characterize the feed. In recent years even nuclear magnetic resonance spectroscopy has been... 

Bromine (128 g., 0.80 mole) is added dropwise to the well-stirred mixture over a period of 40 minutes (Note 4). After all the bromine has been added, the molten mixture is stirred at 80-85° on a steam bath for 1 hour, or until it solidifies if that happens first (Note 5). The complex is added in portions to a well-stirred mixture of 1.3 1. of cracked ice and 100 ml. of concentrated hydrochloric acid in a 2-1. beaker (Note 6). Part of the cold aqueous layer is added to the reaction flask to decompose whatever part of the reaction mixture remains there, and the resulting mixture is added to the beaker. The dark oil that settles out is extracted from the mixture with four 150-ml. portions of ether. The extracts are combined, washed consecutively with 100 ml. of water and 100 ml. of 5% aqueous sodium bicarbonate solution, dried with anhydrous sodium sulfate, and transferred to a short-necked distillation flask. The ether is removed by distillation at atmospheric pressure, and crude 3-bromo-acetophenone is stripped from a few grams of heavy dark residue by distillation at reduced pressure. The colorless distillate is carefully fractionated in a column 20 cm. long and 1.5 cm. in diameter that is filled with Carborundum or Heli-Pak filling. 4 hc combined middle fractions of constant refractive index are taken as 3-l)romoaccto])lu iu)nc weight, 94 -100 g. (70-75%) l).p. 75 76°/0.5 mm. tif 1.57,38 1.5742 m.]). 7 8° (Notes 7 and 8). 

The oil dad rhe characteristic odour of thuja leaf oil, dun to the pre-Eenei of a seir uiir rpeQe the specilic pravit,v was O dO Ll the index o[ refraction, T47Q7 and the specific rolation, — -h 19-26A... 

---