Granulation extruder-granulator

Wet pastes that cannot be granulated or extruded may be predried and preformed on a steam-neated finned drum. Preforming on a finned drum may be desirable also in that some prediying is accomplished. 

The turbo-tray dryer can handle materials from thick slurries [1 million (N s)/m (100,000 cP) and over] to fine powders. It is not suitable for fibrous materials which mat or for doughy or tacky materials. Thin slurries can often be handled by recycle of dry product. Filter-press cakes are granulated before feeding. Thixotropic materials are red directly from a rotary filter by scoring the cake as it leaves the drum. Pastes can be extruded onto the top shelf and subjected to a hot blast of air to make them firm and free-ffowing after one revolution. 

In terms of processing there is no need for pre-drying PCHE granules, a standard extruder screw as used for polycarbonate may be used and discs are said to release well from the mould. Question marks remain on the oxidative stability of the polymer and on the quality of adhesion of the reflective layer but Dow claim that metallising is possible. 

From the third reactor the polymer is then run into a devolatilising ( stripping ) vessel in the form of thin strands. At a temperature of 225°C the solvent, residual monomer and some very low molecular weight polymers are removed, condensed and recycled. The polymer is then fed to extruder units, extruded as filaments, granulated, lubricated and stored to await dispatch. 

The particular features of the nylons should also be taken into account in extrusion. Dry granules must be used unless a devolatilising extruder is employed. Because of the sharp melting point it is found appropriate to use a screw with a very short compression zone. Polymers of the lowest melt viscosity are to be avoided since they are difficult to handle. Provision should be made to initiate cooling immediately the extrudate leaves the die. 

Modified polyphenylene oxides may be extruded, injection moulded and blow moulded without undue difficulty. Predrying of granules is normally only necessary where they have been stored under damp conditions or where an... 

Dried granules may be injection moulded, blow moulded and extruded without undue difficulty with melt temperatures of 220-260°C. The moulding shrinkage (0.003-0.004 cm/cm) is very low and a somewhat greater than normal draft may be required in deep draw moulds. 

If the extruder is coupled to a die which is used to produce two laces for subsequent granulation, calculate the output from the extruder/die combination when the screw speed is 100 rev/min. Each of the holes in the lace die is 1.5 mm diameter and 10 mm long and the viscosity of the melt may be taken as 400 Ns/m. ... 

A lace of polyethylene is extruded with a diameter of 3 mm and a temperature of 190°C. If its centre-line must be cooled to 70°C before it can be granulated effectively, calculate the required length of the water bath if the water temperature is 20°C. The haul-off speed is 0.4 tn/s and it may be assumed that the heat transfer from the plastic to the water is by conduction only. 

In another case where the twin-screw extruder was used, the rubber and plastic were melt mixed with all ingredients in a similar manner as described in blend compositions for static vulcanizations. The product was then dumped, cooled, and granulated. The premixed granules were then fed into a twin-screw extruder where a very narrow temperature profile was maintained with a relative high compression (2 1), and the screw speed was adjusted depending on the final torque and the flow behavior of the extruded stock. The stock was cured by shear force and temperature enforced by the twin-screw extruder. The dynamically crosslinked blend was taken out in the form of a strip or solid rod to determine the... 

On an industrial scale, PA-6 is synthesized from e-caprolactam with water as the initiator. The process is very simple if the reaction is earned out at atmospheric pressure. The polymerization is earned out in a VK-reactor (Fig. 3.23), which is a continuous reactor without a stirrer, with a residence time of 12-24 h at temperatures of 260-280°C.5,28 Molten lactam, initiator (water), and chain terminator (acetic acid) are added at the top and the polymer is discharged at the bottom to an extruder. In this extruder, other ingredients such as stabilizers, whiteners, pigments, and reinforcing fillers are added. The extruded thread is cooled in a water bath and granulated. The resultant PA-6 still contains 9-12%... 

At the bottom of the tower, the high molar mass poly(styrene) is extruded, granulated, and cooled prior to packaging. 

Batch ovens Forced convection Paste, granules, extrude cake Pigment dyestuffs, pharmaceuticals, fibres... 

To a 500 g sample of acidic, dealuminized mordenite (CBV-20A from PQ Corporation, 1.5 mm diameter extrudates that had been calcined at 540 °C, overnight) was added a solution of 33 ml of 48% HF in 1633 ml of distilled water, and the mix cooled in ice, stirred on a rotary evaporator overnight, then filtered to recover the extruded solids. The extrudates were further washed with distilled water, dried in vacuo at 100 °C, and then calcined at 540 °C, overnight. Analyses of the treated mordenite showed 1.2% fluoride, 0.49 meq/g acidity. Samples were charged to the reactive distillation unit either as 20/40 mesh granules, or as ca. 1.5 mm extrudates. 

As the polymer granules enter the melting zone (which we also refer to as the transition zone), their temperature rises and they begin to melt, The heat required to melt the polymer comes from two sources, external heaters and mechanical work from the action of the screw. When we extrude viscous polymers at high rates we may need to cool the barrel to remove some of the heat induced by working the molten polymer. 

In this chapter we have introduced the basic principles underlying polymer extrusion. As we have seen, extruders have two primary purposes they convert polymer granules into a homogeneous molten stream that is pumped to a forming device. The forming devices can take many forms to make a wide variety of continuous products. Among the continuous products made by extrusion are films, pipes, and fibers, which are used in all manner of products that make modern life more convenient and comfortable. Each of the processes that we have described has multiple variants, both major and minor. In each of the sections... 

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