Gas chromatography with atomic emission

Organotin compounds enriched from a diethylether extract of a snow sample collected from the city of Gdansk, Poland and analyzed are shown in Fig. 22 b, c [286]. Gas chromatography with atomic emission detection (GC-AED) run in the chlorine and tin channels, respectively, revealed the presence of tributyltin chloride and this was subsequently confirmed by GC-MS and GC-AED analyses of an internal standard solution (e.g., 1-chlorooctane) of that compound. Quantification was based on the response to chlorine (wavelength 479 nm) in the AED system, and a detection limit of 0.5-1 ng/1 was achieved for all the reference substances. 

Hankemeier TH, Louter AJH, Rinkema FD, et al. 1995. On-line coupling of solid-phase extraction and gas chromatography with atomic emission detection for analysis of trace pollutants in aqueous samples. Chromatographia 40(3-4) 119-124. 

A. M. Carro, I. Neira, R. Rodil and R. A. Lorenzo, Speciation of mercury compounds by gas chromatography with atomic emission detection. Simultaneous optimisation of a headspace solid-phase microextraction and derivatisation procedure by use of chemometric techniques, Chro-matographia, 56(11/12), 2002, 733-738. 

P.L. Wylie, J.J. Sullivan and B.D. Quimby, An investigation of gas chromatography with atomic emission detection for the determination of empirical formulas, J. High. Resolut. Chromatogr., 13, 499-506 (1990). 

J.R. Stuff, W.R. Creasy and A.A. Rodriguez, Gas chromatography with atomic emission detection as an aid in the identification of chemical warfare related materials, 7. Microcol. Sep., 11, 644-651 (1999). 

I. R. Pereiro, A. Wasik, R. -obin ski, Determination of mercury species in tish reference materials by isothermal multicapillary gas chromatography with atomic emission detection after microwave-assisted solubilization and solvent extraction, J. Anal. Atom. Spectrom., 13 (1998), 743D747. 

Liang F, Lu M, Birch ME, et al. Determination of polycyclic aromatic sulfur heterocycles in diesel particulate matter and diesel fuel by gas chromatography with atomic emission detection. J Chromatogr A 2006 1114(1) 145-53. 

Swan, H. B. and Ivey, J. P., Analysis of atmospheric sulfur gases by capillary gas chromatography with atomic emission detection, J. High Resolut. Chromatogr., 17, 814-820, 1994. 

Becker, G., Nilsson, U., Cohnsjo, A., and Ostman, C., Determination of polycyclic aromatic sulfur heterocyclic compounds in airborne particulate by gas chromatography with atomic emission and mass spectrometric detection, J. Chromatogr. A, 825, 57-66, 1998. 

Vinas, P., Campillo, N., Ldperz-Garcia, I., Aguinaga, N., and Hem dez-Cordoba, M., Capillary gas chromatography with atomic emission detection for pesticide analysis in soil samples, J. Agric. Food Chem., 51, 3704-3708, 2003. 

Mothes, S., Popp, P., and Wennrich, R., Analysis of organophosphorus insechcides in natural waters by use of Stir-Bar-Sorphve extrachon then gas chromatography with atomic emission detection, Chromatographia, 57(Suppl.), S/249-S/252, 2003. 

The selective detection of hetero-atom containing organo-compounds is used extensively in the petroleum industry for process control (sulfur, nitrogen, etc.) and additives in fuels (sulfur, nitrogen, oxygen, phosphorous etc.). The most common selective atom detection is performed by gas chromatography with atomic emission (AED) [1-3], sulfur and/or nitrogen chemiluminescence [4—8] and flame photometric (FPD, p-FPD) [9],... 

Recently, a variety of sulfijr- and selenium-bearing compounds were identified through the use of GC/MS techniques [51-53], element specific technique of gas chromatography with atomic emission detection (GC-AED) [54], and by proton-transfer-reaction mass spectrometry (PTR-MS)[55] in the breath of persons after the ingestion of garlic. 

GC-AED Gas chromatography with atomic emission detection GC-FPD Gas chromatography with flame photometric detection GC-MS Gas chromatography-mass spectrometry... 

Campillo, N. Penalver, R. Hernandez, M. (2010). Determination of Dimethylselenide And Dimethyldiselenide in Milk and Milk By-Products by Solid-Phase Microextraction and Gas Chromatography With Atomic Emission Detection. Talanta, Vol.80, pp. 1856-1861, ISSN 00399140. 

Reprinted with permission from Leo et al. (2002) Gas chromatography with atomic emission detection A Powerful technique. Trends in Analytical Chemistry 21(9 10) 618-626 Elsevier. 

Cai XJ, Block E, Uden PC, Sullivan JJ, and Quimby BD (1995) Allium chemistry identification of natural abundance organoselenium compounds in human breath after ingestion of garbc using gas chromatography with atomic emission detection. Journal of Agricultural and Food Chemistry 43 1751-1753. 

Olson, N.L. Carrel, R. Cummings, R.K. Rieck, R. Gas chromatography with atomic emission detection for pesticide screening and confirmation. LC-GC 1994, 12, 142. 

Janak, K. Colmsjb, A. Ostman, C. Quantitative analysis using gas chromatography with atomic emission detection. J. Chromatogr. Sci. 1995, 33, 611. 

Wylie, P. L. and B. D. Quimby, 1989. Applications of gas chromatography with atomic emission detector. 

Struppe C, Schafer B, Engewald W (1997) Nitro musks in cosmetic products - determination by headspace solid-phase microextraction and gas chromatography with atomic-emission detection. Chromatographia 45 138-144... 

Vinas, P. et al.. Determination of pesticides in waters by capillary gas chromatography with atomic emission detection, /. Chromatogr. A, 978, 249,2002. 

Gas Chromatography with Atomic Emission Detection). GC-AED chromatograms of hexane soluble fraction of VGO were also included. Also shown in this figure are the distributions of specific molecular species that must be converted into hydrocarbons by hydrotreating in the presence of partner species. 

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