Flash recovery process

Separation and recovery of the desired fatty acids are difficult from such mixed products, and many recovery processes have been patented. The use of morpholine soaps in separating the acids has been patented. One practical procedure is based on the removal of unreacted hydrocarbons at high temperatures (320°C for soap acids and 380°C for edible acids) by flashing from pressure systems. ... 

Quite apart from the relatively low cost of white spirit and the difficulty of preserving its odour through the recovery process there is a problem in maintaining its flash point and its evaporation rate. 

Catalyst recovery is a major operational problem because rhodium is a cosdy noble metal and every trace must be recovered for an economic process. Several methods have been patented (44—46). The catalyst is often reactivated by heating in the presence of an alcohol. In another technique, water is added to the homogeneous catalyst solution so that the rhodium compounds precipitate. Another way to separate rhodium involves a two-phase Hquid such as the immiscible mixture of octane or cyclohexane and aliphatic alcohols having 4—8 carbon atoms. In a typical instance, the carbonylation reactor is operated so the desired products and other low boiling materials are flash-distilled. The reacting mixture itself may be boiled, or a sidestream can be distilled, returning the heavy ends to the reactor. In either case, the heavier materials tend to accumulate. A part of these materials is separated, then concentrated to leave only the heaviest residues, and treated with the immiscible Hquid pair. The rhodium precipitates and is taken up in anhydride for recycling. 

Cryogenic distillation has been used extensively ia the processiag of natural gas for nitrogen removal and for helium recovery (22—23). Two basic processes are now used for nitrogen rejection from natural gas— the single-column heat-pumped process and the double-column process. Eadier processes utilized multistage flash columns for helium recovery from natural gas (24). 

The steam/process air heater with multiple coils typifies the kind of application on which recovery of flash steam... 

Where high temperatures are required (e.g. for process work) and lower temperatures for space heating, it is desirable to use flash steam recovery from the high-temperature condensate to feed into the low-temperature system, augmented as required by reduced pressure live steam. 

Outlier detection, in chemometrics, 6 56-57 Outokumpu flash smelting, 16 146 Outokumpu lead smelting process, 14 745 Outokumpu Oy process, selenium recovery via, 22 83... 

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