E Solid-State Nuclear Magnetic Resonance

Axelson, D. E., Solid State Nuclear Magnetic Resonance of Fossil Fuels An Experimental Approach, Multiscience Publications, Canada, 1985. 

Bugay, D.E. Solid-state nuclear magnetic resonance spectroscopy theory and pharmaceutical applications. Pharm. Res. 1993, 10, 317-327. 

D.E. Sandstrom, Solid State Nuclear Magnetic Resonance of Synthetic Mineral Surfaces, Thesis, Lulea University of Technology, Lulea, Sweden, 2006. 

R. M. Kowalczyk, T. F. Kemp, D. Walker, K. J. Pike, P. A. Thomas, J. Kreisel, R. Dupree, M. E. Newton, J. V. Flanna and M. E. Smith, A variable temperature solid-state nuclear magnetic resonance, electron paramagnetic resonance and Raman scattering study of molecular dynamics in ferroelectric fluorides. /. Phys. Condens. Matter, 2011, 23, 315402. 

Wilson, M. A., Vassallo, A. M., Perdue, E. M., and Reuter, J. H. (1987). A compositional and solid state nuclear magnetic resonance study of humic and fulvic acid fractions of soil organic matter. Anal. Chem. 59, 551-558. 

Figure 14.1b reproduced with permission from R. Graf, D.E. Demco, S. Hafner and H.W. Spiess, Solid State Nuclear Magnetic Resonance, 1998, 12, 139, Figure 2b. Copyright... 

L. Gasper, D.E. Demco and B. Bliimich, Solid State Nuclear Magnetic Resonance, 1999,14,105. 

Forbes J, Bowers J, Shan X, Moran L, Oldfield E, Moscarello MA, Some new developments in solid-state nuclear magnetic resonance spectroscopic studies of lipids and biological membranes, including the effects of cholesterol in model and natural systems, /. Chem. Soc. Faraday Trans., 84 3821-3849, 1988. 

Plasticisers are added to PVC to achieve flexibility and workability. The flexibility or softness is determined by the type of plasticiser and level used in relation to the PVC (phr). They also operate as an internal lubricant between the PVC molecules. Based on organic esters, e.g., phthalates, adipates, trimellitates, phosphates, etc., addition levels can be as low as 20 phr for semi-rigid to 100 phr for very flexible applications. The effect on the thermal stability significantly depends on the physical state of the PVC-plasticiser system (260). The relative amount of crystalline PVC in PVC/diethylhexyl phthalate has been identified on the basis of a combination of carbon-13 solution and solid state nuclear magnetic resonance (NMR) (361). 

Haase, J. and Oldfield, E. (1994) Solid State Nuclear Magnetic Resonance, 3,... 

Feuerstein M., Engelhard G., McDaniel P. L., MacDougall J. E. and Gaffney T. R., Solid state nuclear magnetic resonance investigation of cation siting in LiNaLSX zeolites. Microporous and Mesoporous Materials 26 (1998) pp. 27-35... 

Moisture was known to increase the mobility of the surface groups of protein as measured by solid-state nuclear magnetic resonance spectroscopy The distribution of water between the protein and the excipients in a freeze-dried powder depends on the crystalline or amorphous nature of the excipients. For example, if a protein is formulated with an amorphous excipient and stored in a sealed container, water would distribute according to the water affinity of the protein and excipients.When the amorphous excipient crystallizes (e.g., because of elevated temperatures), it will expel its sorbed water, which may cause stability problems in the protein. ... 

There are many other characterization methods (e.g., small-angle X-ray scattering, solid-state nuclear magnetic resonance, and Fourier-transformed infrared analysis) for investigating nanocomposite structure. These techniques are extensively reviewed in Ray and Okamoto. ... 

E. Vinogradov. P. K. Madhu and S. Vega, Proton spectroscopy in solid state nuclear magnetic resonance with windowed phase modulated Lee-Goldburg decoupling sequences. Chem. Phys. Lett., 2002, 354, 193-202. 

Analytical techniques commonly used to check for solid-state characteristics include melting point (including hot-stage microscopy), solid-state infrared spectroscopy, x-ray powder diffraction, thermal analysis (e.g., differential scanning calorimetry, thermogravimetric analysis, and differential thermal analysis), Raman spectroscopy, scanning electron microscopy, and solid-state nuclear magnetic resonance (NMR). 

K.J.D. MacKenzie, I.W.M. Brown, R.H. Meinhold, and M.E. Bowden, Outstanding problems in the kaolinite-mullite reaction sequence investigated by silicon-29 and aluminum-27 solid-state nuclear magnetic resonance I, metakaolinite, J. Am. Ceram. Soc. 68(6), 293-297 (1985). 

Solid-State Nuclear Magnetic Resonance Spectroscopy David E. Bugay... 

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