Clogging

Impingement demister systems are designed to intercept liquid particles before the gas outlet. They are usually constructed from wire mesh or metal plates and liquid droplets impinge on the internal surfaces of the mist mats or plate labyrinth as the gas weaves through the system. The intercepted droplets coalesce and move downward under gravity into the liquid phase. The plate type devices or vane packs are used where the inlet stream is dirty as they are much less vulnerable to clogging than the mist mat. 

Allow the reddish-yellow solution to cool to about 40° and then filter off at the pump the polyene which has separated this filtration should be performed as rapidly as possible to avoid contamination with lead acetate, and a Buchner funnel of not less than 6 cm. diameter should therefore be used to avoid clogging the filter. Wash the crude production the filter with... 

Mix 100 g. of ammonium chloride and 266 g. of paraformaldehyde in a 1-litre rovmd-bottomed flask fitted with a long reflux condenser containing a wide inner tube (ca. 2 cm. diameter) the last-named is to avoid clogging the condenser by paraformaldehyde which may sublime. Immerse the flask in an oil bath and gradually raise the temperature. The mixture at the bottom of the flask liquefies between 85° and 105° and a vigorous evolution of carbon dioxide commences at once remove the burner beneath the oil bath and if the reaction becomes too violent remove... 

Vacuum filtering can be a bit tricky, as the filter paper clogs up very quickly and stalls the process. With this stuff it is particularly important to get rid of as much of the solids as possible or your distillation be will very messy. A way round that I have found (that isn t in any book) was to use loads of filter papers, throw them all into a big beaker and then rinse them with solvent, then filter the solvent. Filter tiny amounts at a time, as soon as the paper blocks - stop and change the paper. I normally run the filtrate through at least twice. Any way you can make sure that you have done two... 

One problem with the analysis of salt samples is their tendency to clog the aspirator and burner assembly. What effect would this have on the analysis ... 

Clogging the aspirator and burner assembly decreases the rate of aspiration, decreasing the analyte s concentration in the flame. The result is a decrease in the signal and the introduction of a determinate error. 

Ultrasonic nebulizers are almost free of clogging from solute, have better detection limits, and have become popular despite their high cost relative to the pneumatic forms. A typical construction of an ultrasonic nebulizer is shown in Figure 19.17. 

Jet Aerators. Jet aerators are a cross between the diffused and mechanical aerators. Air and water are pumped separately under the water surface into a mixing chamber and ejected as a jet at the bottom of the tank or pond (Fig. 3f). Jet aerators are suited for deep tanks and have only moderate cost. Disadvantages include high operational costs, limitations caused by tank geometries, and nozzles that can clog. Additionally, they require blowers. 

Filtered valves contain a fine internal filter, typically below the body orifice. This filter prevents clogging by the debris sometimes found in product and package. The use of filtration is recommended with any valve systems containing body, stem, or actuator orifices of 0.25-mm (or smaller) diameter unless exceptional care is taken in the cleaning of product and package components. Valves containing these small orifices are used for products propelled by compressed gas. 

The automation of filter presses has affected several other advantages and developments. Plate shifting mechanisms have been developed, allowing the cloths to be vibrated filter cloth washing, on both sides, has been incorporated to counteract clogging from the expression and downtimes have been reduced with automation, thus increasing capacities. 

The physical property of primary concern in this appHcation is the transmissivity and, depending on the type of installation, the clogging potential and strength properties. 

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