Chromatographic enantioseparations

S. Allenmark, Chromatographic Enantioseparations (Methods and Applications), 2nd Edn, Eliss Horwood Publ. New York, 1991. ISBN 0131329782. 

S. G. Allenmark, Chromatographic Enantioseparations methods and applications, Chichester, Ellis Horwood (1991) 2 Ed. 

Allenmark, S. Chromatographic Enantioseparations Methods and Applications Ellis Horwood New York, 1991. 

Allenmark, S., Chromatographic enantioseparation, Chichester, Ellis Horwood Ltd., 1988 55... 

S. G. Allenmark, "Chromatographic Enantioseparations Methods and Applications", Ellis Norwood, Chichester, UK, 1988. 

Chankvetadze, B., Yamamoto, C., Tanaka, N., Nakanishi, K., Okamoto, Y. (2004). High-performance liquid chromatographic enantioseparations on capillary columns containing monolithic silica modified with cellulose tris(3,5-dimethylphenylcarbamate). J. Sep. Sci. 27, 905-911. 

Allenmark, S. Chromatographic Enantioseparation. Ellis Horwood, Chichester, 1988. 

Petrusevska, K. et al.. Chromatographic enantioseparation of amino acids using a new chiral stationary phase based on a macrocyclic glycopeptide antibiotic, J. Sep. ScL, 29, 1447, 2006. 

Peter, A. et al.. High-performance liquid chromatographic enantioseparation of fS-amino acids, J. Chromatogr. A., 926, 229, 2001. 

Peter, A. et al.. Comparison of column performances in direct high performance hquid chromatographic enantioseparation of 1- or 3-methyl-substituted tetrahy-droisoquinohne analogs. Application of direct and indirect methods, Biomed. Chromatogr, 19, 459, 2005. 

Nimura N, Fujiwara T, Watanabe A, Sekine M, Furuchi T, et al. 2003. A novel chiral thiol reagent for automated precolumn derivatization and high-performance liquid chromatographic enantioseparation of amino acids and its application to the aspartate racemase assay. Anal Bio-chem 315 262-269. 

Lammerhofer, M. and Lindner, W, Recent Developments in Liquid Chromatographic Enantioseparation, In Handbook of Analytical Separations, Valko, K., Ed. Vol 1, Separation Methods in Drug Synthesis and Purification, Elsevier, Amsterdam, pp. 337-426, 2000. 

In addition to the classification of liquid chromatographic enantioseparation methods by technical description, these methods could further be classified according to the chemical structure of the diverse CSPs. The chiral selector moiety varies from large molecules, based on natural or synthetic polymers in which the chirality may be based on chiral subunits (monomers) or intrinsically on the total structure (e.g., helicity or chiral cavity), to low molecular weight molecules which are irreversibly and/or covalently bound to a rigid hard matrix, most often silica gel. 

A selection of the most successful CSPs, chiral particles and chiral additive techniques used for analytical and preparative enantioseparation by LC is discussed in the following sections with respect to molecular recognition and experimental application. As additional sources of background information recent books and review articles2-16, which contain numerous relevant references and examine the most important aspects of the field of liquid chromatographic enantioseparation, should be consulted. 

Allenmark S., Chromatographic Enantioseparation Methods and Applications, 2nd Ed., Ellis Horwood, New York (1991). 

Lammerhofer M, Lindner W, Recent developments in liquid chromatographic enantioseparation, in Separation Methods in Drug Synthesis and Purification, Valko K (Ed.), Elsevier, Amsterdam, Vol. 1, p. 337 (2000). 

Yashima, E. (2001) Polysaccharide-based chiral stationary phases for high-performance liquid chromatographic enantioseparation, J. Chromatogr. A 906, 105-125. 

Yashima, E., Yamamoto, C., and Okamoto, Y. (1996) NMR studies of chiral discrimination relevant to the liquid chromatographic enantioseparation by a cellulose phenylcarbamate derivative, J. Am. Chem. Soc. 118, 4036-4048. 

F. Wang,T. 0 Brien,T. Dowling, G. Bicker, and J. Wyvratt, Unusual effect of column temperature on chromatographic enantioseparation of dihydropyrimidone acid and methyl ester in amylose chiral stationary phase, J. Chromatogr. A 958 (2002), 69-77. 

---