Bis- p-chloroethyl amine hydrochloride

Bis-(P-chloroethyl)amine hydrochloride [821-48-7] M 178.5, m 214-215 . Crystd from Me2CO. [Pg.113]

A solution in dry benzene of 82 grams of bis(p-chloroethyl)amine freshly liberated from its hydrochloride is added gradually to a solution of 36 grams of carbonyl chloride (phosgene) in benzene at a temperature below 10°C. The mixture is mechanically stirred for 3 hours, the precipitate of bis(p-chloroethyl)amine hydrochloride is removed by filtration and the benzene is distilled off on a water bath. The residue is distilled in vacuo and the N-chloroformyl-bis(p-chloroethyl)amine is obtained as a pale yellow oil with a BP of 114° to 116°C at 1 mm Hg. [Pg.1480]

N,N-BIS(2-CHLOROETHYL)AAnNE HYDROCHLORIDE see BHO250 BIS(P-CHLOROETHYL)AMINE HYDROCHLORIDE see BHO250... [Pg.1540]

Bi (P-chloroethyl)amine hydrochloride ]821-48-7] M 178.5, m 214-215 , 216-217", pKEst 5.8 (free base). Crystallise the salt from Me2CO or Me0H/Et20. The picrate has m 112-113" (from EtOH or Me2CO). [Marm J Chem Soc 464 1934, Ward JAm Chem Soc 57 915 1935, Beilstein 4 III 238.]... [Pg.118]

SYNS BIS(P-CHLOROETHYL)AiMINE HYDROCHLORIDE N,N-BIS(2-CHLOROETHYL)AMINE HYDROCHLORIDE BIS(2-CHLOROETHYL)-AMMONIUM CHLORIDE 2-CHLORO-N-(2-CHLOROETHYL)ETHANAMINE HYDROCHLORIDE P,P -DICHLORODIETHYLAMINE HYDROCHLORIDE 2,2 -DICHL0R0DIETHYLAMINE HYDROCHLORIDE DI-2-CHLOROETHYLAMINE HYDROCHLORIDE LEO 72a NC 26 NOR-HN2 NOR-HN2 HYDROCHLORIDE NOR-LOST HYDROCHLORID (GERMAN) NORNITROGEN MUSTARD HYDROCHLORIDE NSC-10873 SK555 TL161... [Pg.178]

N,N-Bis(p-chloroethyl)phosphoric acid amide dichloride N-(2-Chloroethyl)-N-(3-hydroxypropyl)amine hydrochloride Triethylamine... [Pg.3358]

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