Chloroethylamine hydrochloride

Step 4 A solution of 20 grams of the above amino alcohol is dissolved in 50 ml of dry chloroform and treated with dry hydrogen chloride until acid. Then a solution of 9 grams of thionyi chloride in 50 ml of dry chloroform is added and the reaction mixture is heated on a water bath at 50°-60°C for 2 hours. Most of the chloroform is removed by distillation under reduced pressure. Addition of ether to the residue causes the product to crystallize. After recrystallization from a mixture of alcohol and ether, the N-(phenoxyisopropyl)-N-benzyl-0-chloroethylamine hydrochloride melts at 137.5°-140°C. 

C2HftClN 689-98-5) see Fluvoxamine 2-chloroethylamine hydrochloride (C2H7CI2N 870-24-6) see Ifosfamide a-[[(2-chloroetbyl)amino]methyl]benzenemethanol hydrochloride... 

Ethylenimine has been prepared from /8-bromoethylamine hydrobromide by reaction with silver oxide, potassium hydroxide, or sodium methoxide from j3-chloroethylamine hydrochloride by reaction with sodium methoxide or sodium hydroxide and from 8-aminoethylsulfuric acid by reaction with sodium hydroxide. ... 

Banerjee et al. (3) prepared hyperbranched dendrons consisting of polyethyle-neimine and 2-chloroethylamine hydrochloride for use as transfection agents. 

Chloroethylamine hydrochloride, see 2-Chloroethylammonium chloride, 0936 Chloroethylbismuthine, 0888 /V-(2-Chloroethyl)-/V-nitrosocarhamoyl azide, 1128... 

Alkyl and aryl A -substituted 1,2,5-thiadiazolidine-1,1-dioxides 316 are synthesized in good yield from the reaction of sulfuryl chloride with 2-chloroethylamine. 2-Chloroethylamine hydrochloride is heated at 80°C with sulfuryl chloride in acetonitrile, and corresponding mono(chloroalkyl)sulfamyl chloride 314 is then extracted with diethyl ether to separate from unreacted amine hydrochloride. This ether solution is added to a solution of primary amine, and the resultant A -aryl (chloroalkyl)sulfamide 315 is treated with potassium carbonate in DMSO to afford A -substituted 1,2,5-thiadiazolidine-l,1-dioxides 316 <03TL5483>. 

SYNS BIS(P-CHLOROETHYL)AiMINE HYDROCHLORIDE N,N-BIS(2-CHLOROETHYL)AMINE HYDROCHLORIDE BIS(2-CHLOROETHYL)-AMMONIUM CHLORIDE 2-CHLORO-N-(2-CHLOROETHYL)ETHANAMINE HYDROCHLORIDE P,P -DICHLORODIETHYLAMINE HYDROCHLORIDE 2,2 -DICHL0R0DIETHYLAMINE HYDROCHLORIDE DI-2-CHLOROETHYLAMINE HYDROCHLORIDE LEO 72a NC 26 NOR-HN2 NOR-HN2 HYDROCHLORIDE NOR-LOST HYDROCHLORID (GERMAN) NORNITROGEN MUSTARD HYDROCHLORIDE NSC-10873 SK555 TL161... 

NCI-C01661 PHENOXYBENZAMIDE HYDROCHLORIDE N-PHENOXYISOPROPYL-N-BENZYL-P-CHLOROETHYLAMINE HYDROCHLORIDE... 

DICHLOROETHENYL PHOSPHORIC ACID DIMETHYL ESTER see DGP900 DICHLOROETHER see DFJ050 DI-2-CHLOROETHYLAMINE HYDROCHLORIDE see BHO250... 

PHENOXYETHYLDIMETHYLDODECYLAMMONIU M BROMIDE see DXXOOO PHENOXYETHYL ISOBUTYRATE see PDS900 N-PHENOXYISOPROPYL-N-BENZYL-p-CHLOROETHYLAMINE see PDT250 N-2-PHENOXYISOPROPYL-N-BENZYL-CHLOROETHYLAMINE HYDROCHLORIDE see DDG800... 

Potassium thiocyanate (100 g., 1.03 moles) is added to a solution of 115 g. (0.99 mole) of crude /3-chloroethylamine hydrochloride (p. 76) in 200 ml. of water. The resulting solution is refluxed for 9 hours, after which it is cooled and 100 ml. of 40% aqueous sodium hydroxide solution is added. The mixture is extracted with five 300-ml. portions of ether. The combined ethereal solutions are dried over sodium sulfate, and the solvent is removed by distillation, leaving 72 g. (70%) of 2-aminothiazoline, m.p. 76-78°. One recrystallization from benzene gives a product melting at 80-82°. 

Glucosylamino-2-thiazolines (328) are prepared by the reaction of glucosyl isothiocyanates with 2-chloroethylamine hydrochloride (Equation (59)) <92T6413>. 

For the preparation of bis-(2 chloroethylamine) hydrochloride,952 for example, crude diethanolamine hydrochloride (2 moles) is allowed to react with S0C12 (5.33 moles, 388 ml) and benzene (400 ml) at about 30°. 

Aminoethyl chloride hydrochloride. See2-Chloroethylamine hydrochloride... 

Celquat SC-230M Celquat SC-240 Celquat SC-240C. See Polyquaternium-10 2-CEM 50% 2-CEM 70%. See 2-Chloroethylamine hydrochloride CEmCap CEmTex. See Com starch, waxy Centaur 4x6 Centaur 8x30, Centaur ... 

Chloro-1-(3-ethoxy4-nitrophenoxy)-4-(trifluoromethyl) benzene. See Ox luorfen 2-Chloroethyl alcohol p-Chloroethyl alcohol. See Ethylene chlorohydrin 2-Chloroethylamine hydrochloride CAS 870-24-6 EINECS/ELINCS 212-793-2 Synonyms 2-Aminoethyl chloride hydrochloride p-Chloroethylamine hydrochloride 2-Chloroethylammonium chloride... 

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