Tools for Troubleshooting

There are a number of tools that will help during the troubleshooting process. A discussion of a number of the important tools follows. 

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Record the current during the runs, as this is a valuable tool for troubleshooting. It is recommended to avoid current flows higher than 100 pA since the resulting amount of Joule heating may generate system failures. 

A DOS bootable diskette is a valuable tool for troubleshooting. The creation process is very simple. Insert a blank 1.44MB or 720KB diskette into your floppy drive and type the following at a DOS prompt ... 

In addition to the self-tests, you have another tool for troubleshooting HP laser printers. Error codes are a way for the LaserJet to tell the user (and a service technician) what s wrong. Table 10.5 details some of the most common codes displayed on an HP LaserJet. 

As in any scientific document, one must provide a rationale for the parameters chosen and their effect on the overall success of the transfer. This includes an explanation for the system suitability parameters that have been established for the method. System suitability can be a powerful tool for troubleshooting method discrepancies in addition to being a test of the conformance of the system to a set of parameters before analysis. 

An invaluable tool for troubleshooting and maintenance is the instrument control chart. Anything useful can be control charted, such as detector response factors, deviation from expected retention time, etc., but the analysis results from a check gas is one of the most popular items to chart. The most important information a control chart can show is when the instrument needs maintenance or recalibration. While it may seem like a good idea to recalibrate every day, the act of recalibration has error associated with it, and thus overcalibrating can be as much of a problem as undercalibrating. Statistical tools can... 

Given the detailed background of MBP process and other considerations discussed previously, this section aims to provide additional tools for troubleshooting in case a problem arises. The key components of developing MBP depend on three components API, polymer, and process. Troubleshooting needs to be evaluated with respect to its impact on the critical quality attributes as well as the process. Summary of various processes and the key considerations is provided in Table 11.3. 

Nevertheless, these correlations are very practical tools for tracking unit performance and for troubleshooting. They are also important in process design and catalyst research. 

Polymer solution viscosity is a troubleshooting tool for polymer processing. Solution viscosity may be utilized to determine the degradation of some polymers via a decrease in molecular weight, particularly for polymers that can be hydrolyzed by water. It can be a troubleshooting tool because the results can be obtained quite rapidly. Intrinsic viscosity is commonly known as IV when referring to polyesters. It is applicable, however, to any polymer that is soluble at moderate concentrations in a good solvent [2]. 

Several tools are very important for troubleshooting a process. These tools include measuring devices for determining the geometry of the screw, measuring temperature, and collecting process data. Troubleshooting a process without these tools... 

Luckily, there are circuits that fill all of the power requirements listed above and more. SPICE can be an indispensable tool for designing, troubleshooting, and characterizing power conversion circuits. 

Mixer instrumentation, in general, has numerous benefits. In addition to a possible end-point determination, it ean be used to troubleshoot the machine per-formanee (for example, help detect worn-out gears and pulleys or identify mixing and binder irregularities). Instrumentation ean serve as a tool for formulation fingerprinting, assure bateh reproducibility, aid in raw material evaluation, proeess optimization, and scale-up. 

I n addition to learning about the many common problems and troubleshooting techniques for Windows, you should know about the different resources that Microsoft provides with Windows to troubleshoot Windows. These resources are the best to use if you have no other troubleshooting tools available. They can also be used as a starting point for troubleshooting a computer. The built-in Windows tools that the A+ exam tests you on, include ... 

Material balances are also useful tools for the study of plant operation and troubleshooting. They can be used to check performance against design, to extend the often limited data available from the plant instrumentation, to check instrument calibrations, and to locate sources of material loss. Material balances are essential to obtaining high-quality data from laboratory or pilot plants. 

An understanding of the mechanisms of solid-phase extraction (SPE) are crucial for effective methods development. The four mechanisms outlined in Chapter 2 are sufficient for the majority of SPE and are an effective set of tools for methods development. The molecule s structure and the sample matrix are the main features used to choose a mechanism of isolation and separation. This chapter will discuss a six-step approach to methods development, how to execute the SPE recovery experiment, troubleshooting and optimizing conditions for the SPE recovery experiment, and how to critically evaluate previously published methods. 

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