Synthesis and NMR

L., VoLL, G., Haupt, M., Schuster, A., Holzmann, B., and Kessler, H. Synthesis and NMR structure of peptidomi-metic a4/ 7-integrin antagonists. ChemBioChem 2002, 3, 575-578. 

Altoff, W., Fild, M., Rieck, H.-R, and Schmutzler, R., Synthesis and NMR spectroscopic studies of phosphorus compounds with vinyl and ethynyl groups, Chem. Ber., Ill, 1845, 1978. 

Lie and coworkers31 reported the synthesis and NMR properties of all geometrical isomers of conjugated linoleic acids. Pure geometric isomers of conjugated linoleic acid (CLA) were prepared from castor oil as the primary starting material. Methyl octadeca-9Z, 11 /i-dienoate (36) and methyl octadeca-9Z,llZ-dienoate (38) were obtained by zinc reduction of methyl santalbate (35, methyl octadec-11 -en-9-ynoatc) and methyl... 

H. M. I. Osborn and A. Turkson, Synthesis and NMR spectroscopic analysis of 3-nitro-pyranoside, 3-nitro-septanoside and 4-nitro-septanoside derivatives by condensation of the anion of nitromethane with glycoside dialdehydes, Tetrahedron Asymmetry, 20 (2009) 2162-2166. 

R. Albert, K. Dax, S. SekH, H. Stcrk. and A. E. Stutz, S-Deoxy-S-fluoro-D-glneafuranoae and L-iodofuranose synthesis and NMR studies, J. Carbohydr. Chem. 4 513 (1983). 

Ring opening can nevertheless occur. The synthesis and NMR spectroscopy have been described for a series of ring-opened platmacyclopent-4-ene-2,3-dione complexes... 

J. Karban, M. Budesinsky, M. Cerny, and T. Trnka, Synthesis and NMR spectra of l,6-anhydro-2,3-dideoxy-2,3-epimino- and l,6-anhydro-3,4-dideoxy-3,4-epimino-/i-D-hexopyranoses, Collect. Czech. Chem. Commun., 66 (2001) 799-819. 

Cramer N, Buchweitz M et al (2006) Total synthesis and NMR investigations of cyclindra-mide. Chem Eur J 12 2488-2503... 

The synthesis and NMR study of benzo[l,2,3,4]tetrazine 1,3-dioxides have been described <02EJO2342>. A convenient one-pot synthesis and antimicrobial activity of pyrimido[l,2-6][l,2,4,5]tetrazines 68 bearing different substituents have been reported <02JHC45>. 

Gagnaire G, Robert D (1977) A polymer model of lignin (DHP) nC selectively labeled at the benzylic positions synthesis and NMR study Makromol Chem 178 1477-1495... 

P. I. Arvidsson, M. Rueping, D. Seebach, Design, machine synthesis, and NMR-solution structure of a p-heptapeptide ffoming a salt-bridge stabilised 3i4-helix in methanol and in water , Chem. Commun. 2001, 649 - 650. 

Suthers, B.D., Jacobs, M.F., and Kitching, W. 1998. Synthesis and NMR profiling of dioxabicyclo[3.2.1]octanes related to pinnatoxin D. Confirmation of the relative stereochemistry about rings E and F. Tetrahedron Lett. 39, 2621-2624. 

Li, X., Zhang, S., Zhao, P, Kovacs, Z., and Sherry, A.D. (2001) Synthesis and NMR studies of new DOTP-hke lanthanide(III) complexes containing a hydrophobic substiment on one phosphonate side arm. Inorganic Chemistry, 40, 6572-6579. 

Grosjean E., Poinsot J., Charrie-Duhaut A., Tabuteau S., Adam P., Trendel J., Schaeffer P., Connan J., Dessort D., and Albrecht P. (2001) Synthesis and NMR characterization of novel highly cyclised polyprenoid hydrocarbons from sediments. J. Chem. Soc. Perkin Trans. 1, 711-719. 

Eyrisch, O, Sinerius, G, Fessner, W-D, Eacile enzymic de novo synthesis and NMR spectroscopic characterization of D-tagatose 1,6-bisphosphate, Carbohydr. Res., 238, 287-306, 1993. Henderson, I, Sharpless, KB, Wong, C-H, Synthesis of carbohydrates via tandem use of the osmium-catalyzed asymmetric dihydroxylation and enzyme-catalyzed aldol addition reactions, J. Am. Chem. Soc., 116, 558-561, 1994. 

Chattha, M.S., Synthesis and NMR spectrum of diethyl 3-buten-3-methyl-2-oxo-l-phosphonate, Chem. Ind. (London), 1031. 1976. 

Costisella, B., and Gross, H., a-Substituted phosphonates. Part 22. Synthesis and NMR spectra of open-chain and cyclic acetals of formyl phosphonates and formyl diphenylphosphine oxide, J. Prakt. Chem., 319, 8, 1977. 

Sipila, J., and Syrjanen, K. (1995) Synthesis and NMR spectroscopic characterization of six dimeric arylglycerol- 3-aryl ether model compounds representative of syringyl and/7-hydroxyphenyl structures in lignins. On the Aldol reaction in b-ether preparation. Holzforschung 49(4), 325-331. 

Calystegins A3, Bi and B2 (257a-c) were isolated from Calystegia sepium. These alkaloids were also present in Convolvus arvenis and Atropa belladonna, and they were found to be catabolized by Rhizobium meliloti strain 41 [584], The structures of 257a-c were determined with HRMS, and H and NMR, and were confirmed by the synthesis and NMR analysis of model compounds [585], C-Putrescine served as a biosynthetic precursor for the calystegins [586],... 

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