Single source precursors syntheses

Hojamberdiev M, Prasad RM, Fasel C, Riedel R, lonescu E (2013) Single-source-precursor synthesis of soft magnetic FeaSi- and Fe5Si3-containing SiOC ceramic nanocomposites. J Eur Ceram Soc 33(13-14) 2465-2472... 

Linck, C., lonescu, E., Noimenmacher, K., Fasel, C., Kleebe, H. J., Riedel, R. (2013). (Manuscript submitted for publication). Single-source-precursor synthesis of SijNyZrN and SiC/ZrC ultrahigh-temperature stable ceramic nanocomposites. Journal of the American Ceramic Society. 

Malik, M. A. Revaprasadu, N. and O Brien, P. (2001). Air-stable single-source precursors for the synthesis of chalcoeenide semiconductor nanoparticles. Chem. Mater., 13, 913-920. 

Xinglong Wu, Cao M, Changwen Hu, He X (2006) Sonochemical synthesis of prussian blue nanocubes from a single-source precursor. Cryst Growth Design 6(l) 26-28... 

This review has described the synthesis, structure and reactivity of important classes of group 13/15 compounds such as Lewis acid base adducts and heterocycles. In addition, their potential to serve as single source precursors for the deposition of the corresponding binary materials by MOCVD process has been demonstrated. Because of the large number of compounds containing the lighter elements of group 15, N, P and As, these... 

Scheme 6.1. Synthesis of ternary single-source precursors and decomposition to solid state materials.

Banger, K. K. Cowen, J. E. Hepp, A. F. 2001. Synthesis and characterization of the first liquid single-source precursors for the deposition of ternary chalcopyrite (CuInS2) thin film materials. Chem. Mater. 13 3827-3829. 

Hirpo, W. Dhingra, S. Sutorik, A. C. Kanatzidis, M. G. 1993. Synthesis of mixed copper-indium chalcogenolates. Single-source precursors for the photovoltaic materials CuInQ2 (Q = S, Se)./. Am. Chem. Soc. 115 1597-1599. 

Molecular Group 3-5 compounds are currently of considerable interest for two reasons (a) they can serve as volatile low molecular weight single-source precursors for the CVD synthesis of binary and multinary group 3/5 semiconductors with remarkable optoelectronic properties (54), or (b) they are potentially useful cocatalysts for the polymerization reactions of unsaturated organic substrates (55, 56). Various strategies have been employed to synthesize well-defined aggregates. 

Abstract The review summarizes recent studies on the synthesis of M - Sb compounds and their potential application to serve as single-source precursor in MOCVD processes. General reaction pathways for the synthesis of simple Lewis acid-base adducts R3M - ER 3 and heterocycles of the type [R2MSbR 2]x (M = Al, Ga, In) are described. As-formed compounds were studied in detail in MOCVD processes using hot-wall and cold-wall reactors. Advantages as well as problems using single-source precursors are described. 

Single-Source Precursor Method Using Bis- and Multi-Silylated Compounds for the Synthesis of (Periodic) Mesoporous Organosilicas (PMOs)... 

Only very recently have hybrid materials composed of chiral single-source precursors emerged. The difficulties to obtain chiral PMOs or nonperiodic organosilicas composed of single-source precursors, respectively, are at least twofold (1) chiral precursors are not commercially available and their synthesis is often not trivial,... 

Lin, X.Z. Teng, X., and Yang, H. 2003. Direct synthesis of narrowly dispersed silver nanoparticles using a single-source precursor. Langmuir, 19 10081-5. 

---