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Organic-solvent-substituted single crystals

A single-crystal X-ray analysis of orf/to-sulfonyl substituted phenyliodonium imide 467 showed a structure of loosely associated centrosymmetric dimers with a long-range intramolecular I-N and I-O distance of more than 3.0 A, quite unlike the infinite polymeric chains adopted in the solid state for PhINTs [100]. One of the sulfonyl oxygen atoms forms a short intramolecular T--0 secondary bond to the iodine atom with a bond length of 2.667 A. Because of the non-polymeric structure, imide 467 has excellent solubility in common organic solvents. [Pg.113]

See other pages where Organic-solvent-substituted single crystals is mentioned: [Pg.476]    [Pg.476]    [Pg.102]    [Pg.201]    [Pg.343]    [Pg.840]    [Pg.404]    [Pg.584]    [Pg.334]    [Pg.196]    [Pg.122]    [Pg.88]    [Pg.212]    [Pg.238]    [Pg.473]    [Pg.50]    [Pg.234]   


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Crystal organic single

Crystal solvent

Crystallization solvent

Organic substitutes

Single Organic Solvents

Single organisms

Single solvent crystallization

Solvent substitution

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