Methods in NMR Spectroscopy

On-line coupling of separation techniques to NMR has recently been reviewed [459,651-653], and solvent suppression methods in NMR spectroscopy in particular [654],... 

Because the temperature of a realistic nuclear spin system is not at zero degrees absolute, the internal interaction Hamiltonians always contain two parts one is stationary or coherent, the other fluctuating or incoherent, or random. The former part usually determines the positions of the peaks in a spectrum, the latter part governs the dynamics of the system. However, they may become entangled under certain conditions. For spin-1/2 systems, r.f. interactions can be made larger than the internal interactions in most cases, thus the manipulation of the interactions with r.f. pulses is realizable. This is an advantage of NMR over many other spectroscopies. In fact, most experimental methods in NMR spectroscopy correspond to certain manipulations of the internal interactions. For quadrupolar spin systems, the internal... 

See also Diffusion Studied Using NMR Spectroscopy NMR Pulse Sequences Product Operator Formalism in NMR Solvent Suppression Methods in NMR Spectroscopy Two-Dimensional NMR, Methods. 

See also NMR Pulse Sequences Nuclear Overhaus-er Effect Proteins Studied Using NMR Spectroscopy Solvent Suppression Methods in NMR Spectroscopy Structural Chemistry Using NMR Spectroscopy, Organic Molecules Structural Chemistry Using NMR Spectroscopy, Pharmaceuticals Two-Dimensional NMR Methods. 

See also Biofluids Studied By NMR Chromatogra-phy-iR, Appiications Chromatography-MS, Methods Drug Metaboiism Studied Using NMR Spectroscopy Fourier Transformation and Sampiing Theory NMR Data Processing NMR Puise Sequences Soivent Suppression Methods in NMR Spectroscopy. 

Kuhn, L. (ed.) (2013) Hyperpolarization Methods in NMR Spectroscopy, Topics in Current Chemistry, Springer-Verlag Berlin Heidelberg, vol. 338. 

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