Fieser’s Reagents

Perbenzoic acid and monoperphthalic acid are used in the same manner as MCPBA but a fresh solution of these reagents is usually required syntheses for these reagents can also be found in Fieser and Fieser s Reagents for Organic Synthesis. A microtechnique for perbenzoic acid epoxidation has also been described. ... 

Smith, J.G. St Fieser, M. (1990) Fieser and Fieser s Reagents for Organic Synthesis Collective Index for Volumes I-I2. WUey, New York. 

Fieser and Fieser s Reagents for Organic Chemistry, Vols 1 to 15, Wiley-Interscience, NY, 1967 to 1990. 

Chemistry, Organic—Synthesis. 2. Chemical tests and reagents. I. Fieser, Mary A. Peters, 1909-joint author. II. Title. III. Title Fieser and Fieser s Reagents for organic synthesis. 

Fieser s Reagents for Organic Synthesis, Wiley. An alphabetical listing of reagents nsed in syntheis. Began with a single volume in 1967 by Louis and Mary Eieser, followed by updates. Vol. 24, ed. T. Ho, 2008. Available as a set of volumes (1-23) with cumulative index. Not available online. 

A. Hassner and C. Stumer, Organic Syntheses Based on Name Reactions and Unnamed Reactions, Elsevier, Oxford, 1994, p. 100. See also M. Fieser, Fieserand Fieser s Reagents for Organic Synthesis, Vol. 16, Wiley, New York, 1992, p. 362. 

Diazomethane [H2CN2] [334-88-3] M 42.0, m -145°, b -23°. Diazomethane is produced when V-methyl-V-nitroso-amides, e.g. V-methyl-V-nitrosourea, V,V -dimethyl-V,V -dinitrosooxamide, Z)i5-(V-methyl-V-nitroso)terephthalamide or p-toluenesulfonyl-V-methyl-V-nitrosoamide (Diazald), are treated with strong solutions of NaOH or KOH. [Fieser and Fieser s Reagents for Organic Synthesis 1 191 1967, see also 2 102 1969.] It has been commonly prepared from Diazald as it is commercially available, although V-methyl-V-nitrosourea, which is readily prepared and stored below 5° [Arndt Org Synth CoWYolW 461 1943], is also... 

Tetrahedron Lett 30 3927 1989], and has been useful for the synthesis of a wide range of early transition-metal complexes and organometallic compounds [Negishi TskalaasYa Aldrichimica Acta 18 31 1985, see also selected volumes of Fieser Fieser s Reagents for Organic Synthesis],... 

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