Electromagnetic heating devices

Other microwave-assisted parallel processes, for example those involving solid-phase organic synthesis, are discussed in Section 7.1. In the majority of the cases described so far, domestic multimode microwave ovens were used as heating devices, without utilizing specialized reactor equipment. Since reactions in household multimode ovens are notoriously difficult to reproduce due to the lack of temperature and pressure control, pulsed irradiation, uneven electromagnetic field distribution, and the unpredictable formation of hotspots (Section 3.2), in most contemporary published methods dedicated commercially available multimode reactor systems for parallel processing are used. These multivessel rotor systems are described in detail in Section 3.4. 

Industrial applications include coating paper, plastics, and other heat-sensitive materials for the production of electromagnetic shielding devices and mold making. 

Fig. 10. The Groth ZG 5 centrifuge. R, rotor R, stationary shaft T, Teflon seal K, K, chambers for gas scoops S, S2, scoops V, gas supply M, manometer Z, Z2, tapping points for enriched and depleted gas P, P2, vacuum chambers E, electromagnet for eddy current heating Tb, Tb2, temperature measuring devices K, cooling coil and D, D2, labyrinth seals.

Microwaves are electromagnetic radiation placed between infrared radiation and radio frequencies, with wavelengths of 1 mm to 1 m, which corresponds to the frequencies of 300 GHz to 300 MHz, respectively. The extensive application of microwaves in the field of telecommunications means that only specially assigned frequencies are allowed to be allocated for industrial, scientific or medical applications (e.g., most of wavelength of the range between 1 and 25 cm is used for mobile phones, radar and radio-line transmissions). Currently, in order not to cause interference with telecommunication devices, household and industrial microwave ovens (applicators) are operated at either 12.2 cm (2.45 GHz) or 32.7 cm (915 MHz). However, some other frequencies are also available for heating [1]. Most common domestic microwave ovens utilize the frequency of 2.45 GHz, and this may be a reason that all commercially available microwave reactors for chemical use operate at the same frequency. 

Different devices are used to maintain the preset temperature in a mold cabinets, boilers, chambers, baths, infrared heaters, electromagnetic radiation, and so on. In a number of cases, solidification takes place owing to the heat output during the chemical reactions. 

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