Benzenethiol, 2,4,6-tris salt

Dithioalkoxo- and dithiophenoxo-niobium(V) trichlorides [MCl3(SR)2] were obtained from NbCl5 and thiols and benzenethiol respectively.240 The synthesis of tris(benzenedithiolato) complexes was accomplished by reaction of the appropriate metal amide with a mixture of the dithiol and its sodium salt in THF. The structures of (AsPh4)[M(S2C6H4)3]241""243 showed the... 

CdSjC Hg, Benzenethiol, 2,4,6-tris(l,l-dimethylethyl)-, cadmium salt, [138306-14-6], 31 22... 

SCjjHj, Benzenethiol, 2,4,6-tris(l,l-dimethylethyl)-, [961-39-7], 31 159 SF303P6ReC 9H48, Rhenium(l+), tris[l,2-ethanediylbis[dimethylphosphine]-PP ]-, (OC-6-11)-, salt with trifluoromethanesulfonic acid (1 1), [ 154419-20-2],... 

All operations are carried out under a nitrogen atmosphere using thoroughly degassed solvents. The tetraethylammonium salt of tris(Oethyl dithiocarbonato)-ferrate(II),3 [tris(xanthato)ferrate(II), Fe(etxant)3 ], 3.8 g (6.9 mmole) potassium benzenethiolate, KSC6H5, 4.6 g (31 mmole), and tetraphenylphosphonium chloride, [(C6HS)4P]C1, 5.18 g (13.8 mmole) are added to 25 mL acetonitrile, CH3CN, in a 125-mL Erlenmeyer flask. The suspension is boiled for 15 minutes and the contents of the flask are filtered while hot. 

Carboxylic acids, a-bromination of, 55, 31 CARBOXYLIC ACID CHLORIDES, ketones from, 55,122 CARBYLAMINE REACTION, 55, 96 Ceric ammonium nitrate [Ammonium hexa-nitrocerate(IV)], 55,43 Chlorine, 55, 33, 35,63 CHROMIUM TRIOXIDE-PYRIDINE COMPLEX, preparation in situ, 55,84 Cinnamonitrile, a-phenyl- [2-Propeneni-trile, 2,3-diphenyl-], 55, 92 Copper(l) iodide, 55, 105, 123, 124 Copper(I) thiophenoxide [BenzenethioL copper(I) salt], 55, 123 CYCLIZATION, free radical, 55, 57 CYCLOBUTADIENE, 55,43 Cyclobutadienoiron tricarbonyl [Iron, tri-carbonyKp -1,3-cyclo-butadiene)-], 55,43... 

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