Troubleshooting mechanical evaluation

Sohre, J. S., Reliability—Evaluation for Troubleshooting of High-Speed Tiirbomachinery, ASME Petroleum Mechanical Engineering Conference... 

An understanding of the mechanisms of solid-phase extraction (SPE) are crucial for effective methods development. The four mechanisms outlined in Chapter 2 are sufficient for the majority of SPE and are an effective set of tools for methods development. The molecule s structure and the sample matrix are the main features used to choose a mechanism of isolation and separation. This chapter will discuss a six-step approach to methods development, how to execute the SPE recovery experiment, troubleshooting and optimizing conditions for the SPE recovery experiment, and how to critically evaluate previously published methods. 

In this chapter we shall derive and present relationships or formulae that will allow us to predict a cyclone s cut-point diameter, grade-efficiency curve, overall or gross efficiency, and pressure drop on the basis of measurements taken on a geometrically similar cyclone. These formulae should also allow us to evaluate the performance of an operating cyclone and, if necessary, assist us in troubleshooting its design, mechanical condition, or mode of operation. 

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