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The Different Solution Techniques

The simplest technique may be coprecipitation. In this method, a reagent is added to the stock solution that is destabilized and precipitated. Better mixing at a microscopic level is then achieved without mechanical grinding and mixing. Insoluble carboxylates such as citrates, oxalates and carbonates or hydroxides are the most suitable reagents. [Pg.289]

Another procedure is to rapidly dry the solution at a rate that does not allow the elements to segregate. As an example, aerosols can be sprayed through a furnace heated at the reaction temperature of 900°C. This yields spherical submicronic particles that are most suitable to sinterable compacts. Another way is to spray the solution onto a substrate. This is a simple method of thick film deposition. Very ionic species such as nitrates dissolved in water can be sprayed onto a hot substrate. Long-chain carboxylates, soluble in volatile organic solvents, can be deposited as well, even at room temperature. [Pg.289]


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