Synthesis and Techniques

Included for the first time in this section are books and surveys on spectroscopic techniques which are of great use to the organometallic chemist. In addition to the Chemical Society Specialist Periodical Reports on Spectroscopic Properties of Inorganic and Organometallic Compounds (B6.1) and Mass Spectrometry (B6.2), a series of Annual Reviews (volumes 1 or 2) or Reports (volume 3 onwards) on Nuclear Magnetic Resonance Spectroscopy contains surveys of or P NMR results appertaining to organo-transition metal complexes. 

Annual Review (Reports) on NMR Spectroscopy, ed. E. F. Mooney, Academic 

Mooney and P. H. Winson Fluorine-19 Nuclear Magnetic Resonance Spectroscopy, pp. 243-311 (182), esp. pp. 280-293, Organometallics. 

Nixon and A. Pidcock Phosphorus-31 Nuclear Magnetic Resonance Spectroscopy of Coordination Compounds, pp. 345-422 (111). 

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Angelici, R. J., 1977, Synthesis and Technique in Inorganic Chemistry, 2nd ed., Saunders, Philadel-phia. This book provides a useful exercise in vacuum line practice for the newcomer to the field. 

R J. Angelici, Synthesis and Techniques in Inorganic Chemistry , W. B. Saunders, Philadelphia, 1969 Inorg. 

Girolami, G. S., Rauchfuss, T. B., Angelici, R. J. Synthesis and Technique in Inorganic Chemistry—a Laboratory Manual, 3rd edn. University Science Books Sausalito, CA, 1999. 

Angelici, R. J. Synthesis and Technique in Inorganic Chemistry (Saunders, Philadelphia, 1977). 

Adapted from Robert J. Angelid, Synthesis and Technique in Inorganic Chemistry, 1st ed., p. 51. Copyright 1977 Brooks/Col a part of Cengage Learning, Inc. Reproduced by permission. www.cengage.com/permissions.)... 

Girolami GS, Rauchfuss TB, Angelici RJ (1999) Synthesis and technique in inorganic chemistry a laboratory manual, 3 edn. University Science Books, Sausahto, CA... 

Angelici RJ (1969) Synthesis and techniques in inorganic chemistry. Saunders, Philadelphia... 

There are a number of large works in organic chemistry which deal with laboratory synthesis and technique. A very comprehensive German work is Houben-Weyl s Methoden der organischen Chemie (Fig. 34) edited by E. Muller (G. Thieme Verlag, 4th edn., 1952-) of which 16 volumes have been planned, some in several parts. Volume 1 deals with general methods of laboratory practice in organic chemistry, vol. 2 is a summary of analytical... 

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