Simultaneous small- and wide-angle

Paris O, Loidl D, Peterlik H, Muller M, Lichtenegger H, and Fratzl P. The internal structure of single carbon fibers determined by simultaneous small- and wide-angle x-ray scattering. J. Appl. Crystallogr., 2000 33 695-699. 

Description of the Experimental Set-up for Simultaneous Small and Wide Angle X-ray Scattering and Dielectric Spectroscopy (SWD)... 

R.A. J N. Steven, K. Bernd, B. Wim, M.G. R D.G. E Polymer Structure Determination Using Simultaneous Small- and Wide-Angle X-ray Scattering and Differential Scanning Calorimetry (American Chemical Society, 1994), vol. 581, chap. 13, pp. 162-180... 

Butler M F, Donald A M and Ryan A J (1998) Time resolved simultaneous small-and wide-angle X-ray scattering during polyethylene deformation. II. Cold drawing of linear polyethylene. Polymer 39 39-52. 

Butler M F and Donald A M (1998) A real-time simultaneous small- and wide-angle X-ray scattering study of in situ polyethylene deformation at elevated temperatures Macromolecules, 31 6234-6249. 

Butler M F, Donald A M, Bras W, Mant G R, Derbyshire G E and Ryan A J (1995) A Real-Time Simultaneous Small- and Wide-Angle X-ray Scattering Study of lu-Situ Deformation of Isotropic Polyethylene, Macromolecules 28 6383-6393. 

Murthy NS, Grubb DT. Deformation of lamellar structures Simultaneous small- and wide-angle X-ray scattering smdies of polyamide-6. J Polym Sci Polym Phys 2002 40 691-705. 

Wang, Z.-G., Hsiao, B.S., Sirota, E.B., and Srinivas, S. (2000) A simultaneous small-and wide-angle X-ray scattering study of the early stages of melt crystallization in polyethylene. Polymer, 41, 8825. 

Butler MF, Donald AM, Ryan AJ. Time resolved simultaneous small- and wide-angle x-ray scattering during polyethylene defor-mation-II. cold drawing of linear polyethylene. Polymer 1998 39(l) 39-52. 

Figure 11.14 Effect of applied strain on the 002 d-spacing of a PTT fiber drawn at 3.3 x measured by WAXD [76], Reprinted from Polymer, 42, Wu, J., Schultz, J. M., Samon, K. M., Pangelinan, A. B. and Chuah, H. H., In situ study of structure development in poly(trimethylene terephthalate) fibers during stretching by simultaneous synchrotron small- and wide-angle X-ray scattering, 7141-7151, Copyright (2001), with permission from Elsevier Science...

Wu J, Schultz J M, Yeh F, Hsiao B S and Chu B (2000) In situ simultaneous synchrotron small-and wide-angle X-ray scattering measurement of poly(vinylidene fluoride) fibers under deformation, Mocromo/ecules 33 1765-1777. 

Kolb R, Seifert S, Stribeck N and Zachmann H G (2000) Simultaneous measurements of small-and wide-angle X-ray scattering during low speed spinning of poly(propylene) using s3uichrotron radiation, Polj/mer 41 1497-1505. 

Dokter, W.H., Beelen, T.P.M., van Garderen, H.F., et al. Simultaneous monitoring of amorphous and crystalline phases in silicalite precursor gels. An in situ hydrothermal and time-resolved small- and wide-angle X-ray scattering study. /. Appl. Crystallogr. 27 no. 6 (1994) 901-906. 

If the wide angle and small angle experiments are run simultaneously, the timer is not used. For the wide angle experiment, follow steps 2 to 4 and 6 to 9, timing the exposure by clock. 

Fig. 3. Crystalline evolution of triacylglycerols in fat globules of cream. Three-dimensional plots of small- (A) and wide- (B) angle XRD patterns, recorded simultaneously with differential scanning calorimetry (DSC) experiments during heating of cream at 2 C/min from -8 to 50°C. See Figure 1 for other abbreviation.

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