Sieve tray extractors pulsed

Fig. 9.17 Residence times of (a) continuous and (b) drop phase in a liquid pulsed sieve tray extractor according to measurements (squares and crosses) and according to calculations by the dispersion model (drawn lines). Measured and calculated response curves agree well for the continuous phase, but not for the dispersed phase. (From Ref. 14.)...

Siemens-Martin furnace-regenerator, 590 Sieve tray extractors, 483 capacity, 484,487 diameters, 483, 487 efliciency. 483.487 pulsed, 478,483,487 sizing example, 486 Sieve trays, 428 assembly in a tower, 428 comparison with other types, example, 431... 

The Graesser contactor takes an extreme position in the diagram. It has the highest separation efficiency (10 stages per meter) but the lowest capacity (1-2 m/h). The other extremum takes the static sieve tray extractor with only one equilibrium stage per meter and up to 50 m/h capacity. The capacity of a pulsed sieve tray column is as high as 30 m/h with a separation efficiency of 5 to 6 stages per meter. 

There are two different types of energy input in sieve tray or perforated tray columns (Fig. 6-39) in a pulsed sieve tray extractor (PSE) the liquid column is pulsed in a swing tray extractor (STE) fixed sieve trays are mounted on a swinging axis which is driven by an infinitely variable, directly coupled geared motor, including crank shaft and connecting rod. The top and bottom section are expanded to allow the phases to rest and then separate. 

FIG. 23-38 Efficiency and capacity range of small-diameter extractors, 50 to 150 mm diameter. Acetone extracted from water with toluene as the disperse phase, V /V = 1.5. Code AC = agitated cell PPC = pulsed packed column PST = pulsed sieve tray RDC = rotating disk contactor PC = packed column MS = mixer-settler ST = sieve tray. (Stichlmair, Chem. Ing. Tech. 52(3), 253-255 [1980]). 

Pulsing means that either the whole liquid content of a sieve tray column is continually pushed up and down by a piston that moves to and fro, or the whole plate package is moved up and down [3]. Figure 9.5 illustrates the two extractor constructions schematically. They show about the same efficiency... 

The method of calculation introduced in this chapter not only allows an exact determination of the column diameter for nonpulsed sieve tray columns, but also allows a good estimation of the diameters of pulsed and stirred extractors. For the latter, however, more exact specific equations exist for the flooding point, see for example [1,4]. 

Fig. 6.3-4 Typical performance data of ten different extractor designs for the system tolulene/acetone/water. MS mixer-settler, SE static sieve tray column, PC static packed packed column, RDC rotating disc contactor, PSE pulsed sieve tray column, PPC pulsed packed column, RZE agitated cell extractors...

Stagewise contact with controlled coalescence redispersion cycles Tray column Pulsed sieve column. Pulsed Mixer-Settler-cascade, Extraction tower with controlled cycle Scheibel column, ARD-Extractor, Leisibach column, Mixer-Settler cascade ... 

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