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Precursor stacked film

Characteristics of Stacked Precursor Films The new Cu/Sn/Cu/Zn precursors have good lateral uniformity, and the layers consist of small compact grains. The EDX maps in Figure 1.23 show the macroscopic uniformity of the precursor stacks over a 1.4cm area, in terms of the compositional ratios Cu/(Zn + Sn) and Zn/Sn. Both show only small variations, significantly better than those achieved previously [122). In the example shown, the Cu/(Zn + Sn) ratio was 0.80 0.02 and the Zn/... [Pg.35]

Characterization of Annealed CZTS Films Sulfurization of the Cu/Sn/Cu/Zn precursor stacks gave better microscopic uniformity than the previous Cu/Sn/Zn stacks. An SEM image and EDX maps of the Sn and Zn distributions in a film produced from the Cu/Sn/Cu/Zn precursor stack is shown in Figure 1.26. A comparison with Figure 1.23 shows a much more uniform distribution of the elements for the film formed from the four-layer stack precursor. The high degree... [Pg.35]

Additionally, thin-film layers of the catalyst may be deposited on to the surface of the micro channels by sputtering [73] or CVD [63], In the latter case, aluminum isopropoxide, Al[(CH3)2CHO]3, was used as alumina precursor, which was passed through a ready-stacked reactor at 300 °C for 1 h in a flow containing nitrogen and oxygen in addition. The flow direction was subsequently changed and the procedure repeated. [Pg.392]

Sonobe et al. reported the preparation of carbon materials using the interlamellar spaces of montmorillonite as template and polyacrylonitrile, poly(furfuryl alcohol) and poly(vinyl acetate) as carbon precur-They found that carbon precursors were easily graphitised and the obtained carbon materials were two-dimensional film-like graphite, consisting of highly oriented layer planes, which were stacked thin and wide. " Kyotani et al. produced carbons from poly(furfuryl... [Pg.229]


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