Pilot scale columns point

The previous sections have pointed out that mathematical models of the processes must be proved by experiments, or adapted to experimental results with the aid of pilot extractors. For economic reasons, pilot extractors are usually much smaller than large-scale industrial apparatus. Pulsed pilot columns, for example, have a diameter between 30 and 250 mm, whereas industrial-size columns are up to 2500 mm and more in size. Thus, the question arises of whether or not the calculations or pilot experiments may be used for the dimensions of large-scale apparatus. This is a general problem for engineers. 

The design of a multi-purpose plant for the continuous extraction of liquids with supercritical fluids is presented. To provide flexibility in order to treat different feedstocks, a modular concept was developed based on experience gained in the operation of bench-scale and pilot plants. Four test systems were chosen in order to determine the proper dimensions for the equipment. Based on experimental data, e.g. measurements of flooding points and maximum flows for various column internals, the design pressure and temperature and heat exchange requirements were determined. The plant was built by a German manufacturer and was operated successfully by a Canadian company in Edmonton, Alberta. 

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