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Oleyl-polymethacrylic acid resin

Fig. 3. Preparation of the oleyl-polymethacrylic acid resin. Commercial polymethacrylic acid resin (Amberlite CG 50 III) was refluxed with thionylchloride the excess thionylchloride was removed the partially chlorinated, partially anhydrated resin was suspended in dichloro-methane and oleylamine and triethylamine were added. The resulting resin contained 3.6 meq/g COOH, 66.3% C, 9.6% H, and 2.2%... Fig. 3. Preparation of the oleyl-polymethacrylic acid resin. Commercial polymethacrylic acid resin (Amberlite CG 50 III) was refluxed with thionylchloride the excess thionylchloride was removed the partially chlorinated, partially anhydrated resin was suspended in dichloro-methane and oleylamine and triethylamine were added. The resulting resin contained 3.6 meq/g COOH, 66.3% C, 9.6% H, and 2.2%...
Fig. 4. Chromatographic separation of mitochondrial membrane proteins on oleyl-polymethacrylic acid resin. The chromatography was performed with double-labeled mitochondrial membrane proteins. [ CJleucine was incorporated in the absence and [ H]-leucine in the presence of cycloheximide. The specific C radioactivity of proteins was 94 counts X min x (Mg protein)" For detail see ref. 22. Fig. 4. Chromatographic separation of mitochondrial membrane proteins on oleyl-polymethacrylic acid resin. The chromatography was performed with double-labeled mitochondrial membrane proteins. [ CJleucine was incorporated in the absence and [ H]-leucine in the presence of cycloheximide. The specific C radioactivity of proteins was 94 counts X min x (Mg protein)" For detail see ref. 22.

See also in sourсe #XX -- [ Pg.129 ]




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