Modulated differential scanning

P. S. Gill, S. R. Sauerbrunn, M. Reading. Modulated Differential Scanning Calorimetry. J. Thermal Anal. 1993, 40, 931-939. [Pg.260]

M. Reading. Modulated Differential Scanning Calorimetry—A New Way Forward in Materials Characterization. Trends Polym. Sci. 1993,1, 248-253. [Pg.260]

Study of Polymer Glasses by Modulated Differential Scanning Calorimetry in the Undergraduate Physical Chemistry Laboratory 126... [Pg.130]

The differential scanning calorimeter (DSC) works on a technique that detects physicochemical transition in a system by measuring the amount of heat absorbed or released as the sample is heat across its suspected transition range. The heat absorbed or released from a sample of known mass compared with that of an empty reference pan. Modulated differential scanning calorimeter (mDSC) works on an advanced technology version of DSC, where the signal quality has been improved using... [Pg.516]

Vasanthavada, M., Z. V fong, Y. Joshi, and M. S. Kislalioglu. 2002. Comparison of the utility of thermally stimulated current and modulated differential scanning calorimeter to study sub-glass transition molecular motions of poly(vinylpyrrolidone). Paper presented at AAPS Annual Meeting, Toronto, October 8, 2002. [Pg.528]

The compositions of the composites were determined simply by weighing the tared solid sample. Melting endotherms and glass transition temperatures were determined using a TA Instruments 2910 modulated differential scanning calorimeter (DSC) operated with a 3°C/min ramp rate, a 0.75 °C oscillation amplitude, and a 60-s oscillation period. [Pg.166]

Figure 18.12. Example heat flow behavior of temperature-modulated differential scanning calorimetry. Reproduced from Young and LeBoeuf (2000), by permission of the American Chemical Society.

Figure 18.17. Temperature-modulated differential scanning calorimetry scan of poly(methyl methacrylate) indicating P-relaxation near 32°C and a relaxation (Tg) near 121 °C. Reproduced from DeLapp et al. (2004), by permission of Elsevier, Ltd.

TABLE 18.4. Select NOM Characterization Studies by Differential Scanning Calorimetry (DSC) and Temperature-Modulated Differential Scanning Calorimetry (TMDSC)... [Pg.816]

Hutchinson, J. M. (1998). Characterising the glass transition and relaxation kinetics by conventional and temperature-modulated differential scanning calorimetry. Thermochimica Acta 324(1-2), 165-174. [Pg.831]

Schawe, J. E. K. (1998). A description of the glass transition measured by temperature modulated differential scanning calorimetry. Colloid Polym. Sci. 276(7), 565-569. [Pg.834]

In this section, some case studies will be presented on the characterization of CMP pad and slurry [17-20] using such advanced analytical techniques as dynamic mechanical analysis (DMA), modulated differential scanning calorimetry (MDSC), thermal gravimetric analysis (TGA), thermal mechanical analysis (TMA), dynamic rheometry, dual emission laser induced fluorescence (DELIF), and the dynamic nuclear magnetic resonance (DNMR). More specifically, these techniques were used to characterize (a) the effect of heat... [Pg.32]

Readings, M. (1993). Modulated differential scanning calorimetry—a new way forward in material characterization. Trends Polym. ScL, 1, 248-53. [108]... [Pg.378]

Dielectric relaxation, temperature-modulated differential scanning calorimetry (TMDSC), and H NMR spectroscopy (see Section 4.05.3.2.1) have been used to perform the dynamic characterization of fananserine 35. The use of these three different techniques gives a coherent set of information and allowed the authors to describe the dynamic properties over a wide range of frequencies and temperatures <2006MI798>. [Pg.563]

Varma-Nair, M. Wunderlich, B. Nonisothermal heat capacities and chemical reactions using a modulated differential scanning calorimeter. J. Therm. Anal. 1996, 46, 879-892. [Pg.404]

Hill, V.L. Craig, D.Q.M. Feely, L.C. Characterisation of spray-dried lactose using modulated differential scanning calorimetry. Int. J. Pharm. 1998, 161, 95-107. [Pg.404]

Gill, P.S. Sauerbrunn, S.R. Reading, M. Modulated differential scanning calorimetry. J. Thermal. Anal. 1993,... [Pg.3748]

McPhillips H, Craig DQM. Royal 1 P, ei al. Characterisation of the glass transition behaviour of HPMC using modulated differential scanning calorimetry. Int J Pharm 1999 180 83-90. [Pg.427]

Rabel SR, Jona JA, Maurin MB. Applications of modulated differential scanning calorimetry in performulation studies. J Pharm Biomed Anal 21(2) 339-345,1999. [Pg.576]

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