4-Methyl-2,3,5,6-tetranitro

In befriedigenden Ausbeuten (40 47%) lassen sich 3,5-Dinitro-4-methyl- bzw. 4-Methyl-2,3,5,6-tetranitro-anilin mit Nitriersaure in Pentanitro-anilin iiberfuhren1 ... [Pg.343]

It was prepd in 1884 by Nolting and Collin (Ref 2) from ethyl- or methyl-esters of Styphnic Acid and ale ammonia. Blanksma (Ref 3) prepd it from 3-chlor-2,4,6-trinitroanisole (or 3-chlbr-2,4,6-trinit,rophetietole) and ale ammonia, Kbrner and Contardi ( Ref 4) from 2,4-dibrom- (or dichlor)- 3,5-trinitrobenzene and ale ammonia, and Fliirscheim (Ref 5) from tetranitro-aniline and ammonia... [Pg.717]

Nitro-2-athoxycarbonyl- 694 2 -Nitro-2-carboxy- 694 2-Nitro-2 -formyl- 693 Octachlor-4,4 -bis-[trichlor-vinyl]- 62 7 Octachlor-4,4 -diathinyl- 627 Octachlor-4 -(trichlor-vinyl)-4-athinyl- 627 2,2, 6,6 -Tetrakis-[hydroxyamino]- 695 2,2, 6,6 -Tetranitro- 695 2,2, 4,4 -Tetranitro-6.6 -dicarboxy- 689 4,4, 6,6 -Tetranitro-2,2 -dicarboxy- 660 2-(Trichlorsilyl-methyl)- 555... [Pg.976]

Much more promising is the method of Schechter and Haller (3), which depends upon the coupling of the tetranitro derivative of DDT with methanolic sodium methylate. Under conditions of intensive nitration methoxychlor will yield by this procedure a red color with an absorption maximum at 535 m/z. [Pg.260]

Synonyms BRN 0964788 CCRIS 3143 CE EINECS 207-531-9 7V-Methyl-2,4,6-tetranitro-aniline -Methyl-iV,2,4,6-tetranitrobenzenaniine Nitramine NSC 2166 Picrylmethyl-nitramine Picrylnitromethylamine Tetralit Tetralite Tetril 2,4,6-Tetryl Trinitrophenylmethyl-nitramine Trinitrophenyl-7V-methylnitramine 2,4,6-Trinitrophenylmethylnitramine 2,4,6-Trinitro-phenyl-A7methylnitramine UN 0208. [Pg.1046]

Also called 2,6-Dinitro-4-Picrylaminephenol in Ger). (O, N)3C6H2NHC6H2(N02)20H mw 410.22, N 20.49%, OB to C02 -62.4% ochre-yel crystals (from HAc), mp 248° insol in water, si sol in ale sol in alkalis with formation of a deep-brown color. Prepd by heating picryl chloride, isopicraminic acid NaAc in aq ale. No explosive props are mentioned for it nor for the tetranitro derivatives (Ref 2). The Na salt, of the pentanitro derivative NaCi2HsOuN6, red platelets, explodes above 300°. The 3 -Hydroxy-4-methyl-pentanitro diphenylamine is not explosive (Ref 3)... [Pg.240]

C3H5.HNC6H2(N02)2-C6H2(N02)2NH.C3H5 mw 444.36, N 18.91%, orn-red ndls (from phenol or salicylic acid methyl ester), mp 205° (dec) was prepd by heating at 100° in a sealed tube 3, 5, 31, 51-tetranitro-4, 4 -dimethaxy (or diethoxy) -diphenyl with allylamine in alcohol (Refs 1 3)... [Pg.17]

Tetranitro-3 methylnitramino-di phenyl-amine, also called in Beil N-Nitro-N-methyl-N -[2-nitro-phenyl)-2,4.6 trinitropbenylendia-min-( 1.3), 0JN-CiH4.NH-C6H(N0a)J-N(N02).CHs. Yel crysts (from AcOH), mp 200°(dec). Was prepd by treating 2,4,6-tr ini tro-3-me th y Ini tramino-diphenylamine with HNO,(d 1.49) at RT. Its expl props were not examined... [Pg.230]

Tetranitro-3-methylnitramino-diphenyl-amine, also called in Beil N[ -Nitro-N-metbyl-N3-( 4 nitro-phen.yl)- 2,4- 6-trinitro-phenylendia--min-(13). 0lN-C6H4 NH.C6H(N02)J.N(N0a).CH3. Ot ange-yel crystsffrom AcOH), mp 200°. Was prepd by treating methyl-(2,3,4,6-tetra-nitrophenyI nitramine with 4-nitroaniline in boiling benz. [Pg.230]

Tetranitro-N-methyl-diphenylamine or l-(21,4 - Dini tro-N-me thy lan ilino)-(2,4-dinitrobenzene), (OaN)iCsH3.N(CH3). C8H3-(NOa)a yel leafletsffrom ale or AcOH), mp 210° was prepd by nitrating 2,4-dinitro-N-methyl-diphenylamine as described in Ref 2. Its expt props were not examined... [Pg.439]

Tetranitro-3-methyl-diphenyl-amine, or N-(21,4 -Dinitropkenyl)-4J6-dinitro-m-toluidine, (02N)2C H,.NH.C6Ha(NOa)a.CHs-t yel plates (from AcOH), mp 208-9°. Was obtained on heating on a water bath 3-methyl-21,4 -dinitrodiphenylamine with coned HaS04 and HN03(d 1.42) until the soln became pale yel (ca A hr). Its expl props were not examined... [Pg.440]

Ethylmethylbiimidazole and derivs 6 E311 4-ethyl-4 -methyl-1,1, 5,5 -tetranitro-2,2 -biimidiazole 6 E311... [Pg.610]

Tetryl (2,4,6 -Trinitrophenylmethylnitramine, N-2,4,6-tetranitro-N-methyl aniline, or picrylmethyl-nitramine, also called Pyronite, Tetrylit, Tetra-Ute or Tetralita)... [Pg.642]

Scope. The three major military expls (TNT, RDX and HMX), the four most important military proplnt materials (Nitrocellulose, Nitroglycerin, Nitroguanidine and Dinitrotoluene) and two volatile and expl by-products (Tetranitro-methane from TNT manufg and Methyl nitrate from RDX/HMX manufg) are discussed here. [Pg.826]

Tetranitro-3-methylnitramino-dipheny. amine, also called in Beil N-Nitro-N-methyl-N [2-nitro-phenyh]-2.4.6-trinitropbenylendia-min-(1.3), 02N-C6H4.NH-CtH(N02 )s-N(NOa )-CH3. [Pg.230]

Tetranitro-2-methyldiphenylamine or N-(2, 4 -Dinitrophenyl)-4,6- dinitro-o-toluidine, (02N)2C8H3,NH. C6H2(CH3)(N02)2 yel ndls, mp 190° Can be prepd by heating, on a steam bath, 2 4 -dinitro-2-methyl-diphenyl amine with a mixt of glacial AcOH and nitric acid (dl.42) until a straw colored soln is obtained (ca A hr). Its expl props were not examined... [Pg.440]

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