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4-methoxyphenyl 2-oxo-2-phenylethyl

Methoxyphenyl 2-Oxo-2-phenylethyl Tellurium Dichloride1 0.34 g (1 mmol) of 4-mcthoxyphenyl tellurium trichloride and 0.36 g (3 mmol) of methyl phenyl ketone are intimately mixed and allowed to stand for 48 h. During this time the product crystallizes. Diethyl ether is added to the mixture which is then shaken thoroughly. The ether is decanted, the crystals are quickly washed with a small amount of cold methanol, and recrystallized from benzene/petroleum ether (b.p. 50-70°) yield 0.25 g (60%) m.p. 137". [Pg.544]


See also in sourсe #XX -- [ Pg.544 , Pg.546 ]

See also in sourсe #XX -- [ Pg.430 , Pg.544 , Pg.546 ]




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