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Melting point determination: technique mixed

Molten salt synthesis based on the use of salts with low melting point has been reported to be one of the simplest techniques for preparing ceramic materials [57]. Well-faced LNM crystals were synthesized by molten salt technology using stoichiometric amount of LiOH, Ni(OH)2, and y-MnOOH (2 1 3) calcined at 700-1000 °C [57]. Micro-sized LNM crystals in plate and octahedral shapes were synthesized by molten-salt method in LiCl and LiCl-KCl fluxes the main surface facets on the plates were determined to be (112) crystal planes [58]. Recenfly, microscale LNM was synthesized using nanothom stmctured MnOa mixed with Li and Ni precursors [59]. [Pg.483]


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See also in sourсe #XX -- [ Pg.240 ]




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