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Heptyl acetate

The combined product is mixed with i 1. of 20 per cent sodium hydroxide solution and stirred on the steam bath for four hours, in order to hydrolyze a small proportion of heptyl acetate. The oil is then separated and distilled, and the portion boiling at 172-176° collected. The residue in the flask is mixed with about 100 cc. of water and distilled, whereupon a further small quantity of oil passes over with the steam. This distillate and the forerun are freed of the bulk of the water in a separatory funnel, and distilled from a smaller flask. In this way the total yield of -heptyl alcohol boiling at 172-176° (uncorr.) is 350-370 g. (75-81 per cent of the theoretical amount). The alcohol may be redistilled under reduced pressure, and it passes over almost without loss at 7i-72°/i2 mm. [Pg.52]

They measured the distribution coefficient of n-pentanol between water and mixtures of -heptane and chloroheptane, -heptane and toluene, and n-heptane and heptyl acetate. The two phase system was thermostatted at 25°C and, after equilibrium had... [Pg.109]

Dipolar cycloadditkm reactions of nitrones to olefins, 46, 1,3-Dipolar cycloadditions with 3-phenylsydnone, 45, 98 Dispiro[5 1 5 l]tetradecane-7,14-dione, photolysis to cyclohexylidene-cyclohexane, 47, 34 preparation from cyclohexanecarbonyl chlonde and triethylamine, 47,34 Displacement of bromine from 1-bromo-2-fluoroheptane to give 2-fluoro-heptyl acetate, 46, 37... [Pg.128]

Displacement of bromine from 1-bromo-2-fluoroheptane to give 2-fluoro-heptyl acetate, 46, 37... [Pg.71]

Heptadecyl alcohol 3-Heptanol n-Heptyl acetate n-Hexyl ether Isoamyl acetate Methylbenzylamine... [Pg.219]

C10H20 2,4,6-trimethyl-3-heptene, isomer 123434-07-1 439.96 38.146 2 21046 C10H2002 6-methyl-2-heptyl acetate 67952-57-2 460.15 40.069 1,2... [Pg.500]


See other pages where Heptyl acetate is mentioned: [Pg.251]    [Pg.109]    [Pg.251]    [Pg.1254]    [Pg.621]    [Pg.251]    [Pg.106]    [Pg.648]    [Pg.1352]    [Pg.17]    [Pg.17]    [Pg.88]    [Pg.88]    [Pg.1352]    [Pg.614]    [Pg.51]    [Pg.52]    [Pg.80]    [Pg.27]    [Pg.52]    [Pg.52]    [Pg.59]    [Pg.59]    [Pg.155]    [Pg.155]    [Pg.162]    [Pg.162]    [Pg.247]    [Pg.357]    [Pg.358]    [Pg.365]    [Pg.365]    [Pg.487]    [Pg.487]    [Pg.500]    [Pg.573]   
See also in sourсe #XX -- [ Pg.229 ]

See also in sourсe #XX -- [ Pg.158 ]




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Heptylate

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