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Grignard reactions 272 INDEX

Properties Colorless to pale-yellow liquid. Bp 230C, d 1.439 (25/25C), refr index 1.5414 (20C), flash p 255F (124C) (COC). Readily hydrolyzed with liberation of hydrogen chloride. Combustible. Derivation By Grignard reaction of silicon tetrachloride and chlorophenylmagnesium chloride. Grade Technical. [Pg.288]

Indexes in Collected Volumes I-X under Grignard Reactions. [Pg.321]

Added importance centers on the dialkyldialkoxysilanes in view of the fact that they are satisfactory intermediates for the manufacture of silicon resins. These compounds may be made by a modification of the Grignard method without the use of ether as a solvent,58 and many of the alkyltriethoxysilanes listed in the compound index at the end of this chapter also were made this way.69 The allyltri-ethoxysilane so prepared apparently did not polymerize, but the phenylethynylsilanes prepared by the following reactions... [Pg.38]

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