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Experimental details materials and procedures

After drying PET for 12 hours at 100 C, it was tumble mixed with PP at a constant weight ratio of 15/85. The mixture was then melt blended in a single-screw extruder (Screw diameter 20 mm, L/D ratio 30) using a set temperature profile of 225°C, 235 C, 250°C, 255°C, and 260 C, and the screw rotating at 30 rpm. The extrudate was in the form of [Pg.528]

A JEOL JSM 840 SEM with an acceleration voltage of 20 kV was used for studying the surface morphology of the specimens. To extract the PET component from the specimens, a mixture of phenol/l,l,2,2-tetrachloroethane in 60/40 wt% was used as the solvent. Similarly, to remove PP and retain the PET fibrils, the specimens were treated with hot xylene. AH the specimens were coated with a thin gold layer prior to SEM analysis. The diameters of about 100 fibrils were measured from the micrographs of stretched samples using image analysis software. [Pg.531]

Thermal properties of PP, neat blend, MFBs and MFCs were studied using a Mettler Toledo DSC 822 at a heating and coohng rate of 5°C/min. The samples were heated up to a maximum temperature of 200°C, held there for 3 min, and then allowed to cool to room temperature to analyze the non-isothermal crystallization behavior of PP component. [Pg.531]


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