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Dimethylaminoethyl Chloride Hydrochloride

A solution of 219 g (1 mol) of a-(p-chlorophenyl)-2-pyridinemethanol in one liter of dry toluene is heated to 100°C with stirring. Twenty-three grams (1 g-atom) of sodium are then added in portions. After all the sodium has reacted, a dried solution of 2-dimethylaminoethyl chloride in benzene is added. This benzene solution is prepared by dissolving 173 g (1.2 mols) of 2-dimethylaminoethyl chloride hydrochloride in the minimum amount of water, adding 500 cc of benzene followed by 300 g of sodium carbonate decahydrate, stirring, separating the benzene layer and drying. [Pg.836]

P-DIMETHYLAMINOETHYL CHLORIDE HYDROCHLORIDE (Ethylamine, 2-chloro-N,N-dimethyl-, hydrochloride)... [Pg.37]

A group of amine salts having the formula RC1 HC1, when R represents such groups as (CH3)2NCH2CH2 ((3-dimethylaminoethyl chloride hydrochloride), (CH3)2NCH2CH(CH3) ((3-dimethy-laminoisopropyl chloride hydrochloride), etc. Used in organic synthesis. [Pg.383]

See di(p-chlorophenyl)ethanol. (2) Abbreviation for (3-dimethylaminoethyl chloride hydrochloride. [Pg.476]

A soln. of 1 mole benzylphenylcarbinol in dry benzene added to a stirred suspension of 2 moles NaNH2 in dry benzene, warmed 2hrs. at 60-70° with stirring, -dimethylaminoethyl chloride hydrochloride added, and heated 18 hrs. at 90-95° with stirring —> yS-di-methylaminoethyl 1,2-diphenylethyl ether hydrochloride. Y 69%. (F. e. s. J. B. Wright, H. G. Kolloff, and J. H. Hunter, Am. Soe. 70, 3098 (1948).)... [Pg.77]

Chloro-2-dimethylaminoethane hydrochloride. See Dimethylaminoethyl chloride hydrochloride... [Pg.888]

Trade Name Synonyms Quantacure DMB [Aceto http //www.aceto.com], Xincure DMB [Changzhou Xinghui http //www.xinghuichem. com] Dimethylaminoethyl chloride hydrochloride CAS 4584-46-7 EINECS/ELINCS 224-970-1 Synonyms 1 -Chloro-2-dimethylaminoethane hydrochloride 2-Chloro-N,N-dimethylethylamine hydrochloride N-(2-Chloroethyl) dimethylamine hydrochloride 2-Chloroethyldimethylammonium chloride 2-... [Pg.1396]

Dimethylaminoethyl chloride hydrochloride Dimethyl (2-chloroethyl) amine hydrochloride Dimethyl-P-chloroethylamine hydrochloride DMC... [Pg.1396]

Dimethylaminoethyl chloride hydrochloride intermediate, organic dyes Morpholine a-Picoline intermediate, organic insecticides Morpholine... [Pg.5404]

Dimethylaminoethyl chloride hydrochloride C4Hiod2Si Diethyidichlorosilane C4H10KO... [Pg.7033]

Figure 4.7 Chromatograms from selected ion monitoring (a) VA-dimethylaminoethyl chloride (DMC), 200 pg corresponding to 0.2 ppm, operator 1 (b) dimethylaziridinium (DMA), 1 ng corresponding to 1 ppm, operator 1 (c) DMC, 200 pg, operator 2 (d) batch of diltiazem hydrochloride estimated to contain 0.06 ppm DMC (operator 1). Normal day-to-day variation in retention times is illustrated DMA elutes later than DMC (Rs = 1.6). Reproduced from [22] by permission of the Royal Society of Chemistry. Figure 4.7 Chromatograms from selected ion monitoring (a) VA-dimethylaminoethyl chloride (DMC), 200 pg corresponding to 0.2 ppm, operator 1 (b) dimethylaziridinium (DMA), 1 ng corresponding to 1 ppm, operator 1 (c) DMC, 200 pg, operator 2 (d) batch of diltiazem hydrochloride estimated to contain 0.06 ppm DMC (operator 1). Normal day-to-day variation in retention times is illustrated DMA elutes later than DMC (Rs = 1.6). Reproduced from [22] by permission of the Royal Society of Chemistry.
CH2CH2C02CH2Ph l-Ethyl-3-phenyl p-toluenesulfonate l-(2-Dimethylaminoethyl)-2,3-diphenyl chloride hydrochloride Hemiethanolate... [Pg.258]

See other pages where Dimethylaminoethyl Chloride Hydrochloride is mentioned: [Pg.37]    [Pg.84]    [Pg.56]    [Pg.2729]    [Pg.37]    [Pg.39]    [Pg.55]    [Pg.443]    [Pg.83]    [Pg.84]    [Pg.1223]    [Pg.975]    [Pg.2365]    [Pg.1562]    [Pg.4824]    [Pg.6221]    [Pg.6847]    [Pg.120]    [Pg.258]    [Pg.227]   
See also in sourсe #XX -- [ Pg.31 , Pg.37 ]

See also in sourсe #XX -- [ Pg.31 , Pg.37 ]

See also in sourсe #XX -- [ Pg.31 , Pg.37 ]



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2- dimethylaminoethyl

2-Dimethylaminoethyl chloride

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