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Degradation During Thermal Annealing

Poly(styrene) is fairly temperature stable in contrast to PLA which starts to thermally degrade at 180°C even under an inert atmosphere [31, 32, 51]. The thermal [Pg.61]

4 Voided Double-Gyroid Thin Film Templates [Pg.62]

Theoretical volume fraction of PLA assuming /Jpla = 1.18gcm .  [Pg.63]

The observed inconsistencies are most likely do to varying levels of impurities such as copper salts or monomers. Curiously, degraded films produced bubbles during immersion in the etching solution. The protection of the hydroxyl end-group [Pg.63]


Fig. 4.1 Preparation of mesoporous thin film polymer templates on suitable substrates, a Substrate surface modification tailoring a neutral surface, b Copolymer film deposition and phase transition to the double-gyroid morphology during thermal annealing, c Selective degradation of PLA yields the mesoporous template... Fig. 4.1 Preparation of mesoporous thin film polymer templates on suitable substrates, a Substrate surface modification tailoring a neutral surface, b Copolymer film deposition and phase transition to the double-gyroid morphology during thermal annealing, c Selective degradation of PLA yields the mesoporous template...

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