Chloro phenetole

Chloro- -phenetidine 4-Chloro-o-amino-phenetole, Chloro-2-aminophenffl ethyl ether)... 

Chloro-p-phenetidine (2-CUoro-p-amino. phenetole, 2-(MorO i-ominophmyl ethyl dher). 

The purpose of this experiment was to show the applicability of normal-phase gradients to LC separations. In what was described as a random selection of 10 analytes (2-phenylethylbromide, 1,4-diphenylbutane, phenetole, nitrobenzene, chloro-stilbene oxide, Sudan red 7B, 4-chIorobenzophenone, veratrole, acetophenone, phthalic acid bis-2-ethylhexylester) all peaks were well resolved with good peak shape on a silica column (2 = 254 nm). A two-ramp 100/0 (hold 2 min) 50/50 (at 8.5 min hold 5 min)0/100 (at 20min) hexane/dichloromethane gradient was used [600]. Methyl r-butyl ether was used in place of dichloromethane but resolution was not as good. 

Ethyl Acetoacetate continued) o-Chloro toluene p-Chloro toluene Anisole o-Cresol Styrene Acetophenone Phenyl acetate m-Xylene o-Xylene p-Xylene p-Methylanisole Phenetole Veratrole Methylheptenone Butyl butyrate Isoamyl propionate Butyl ether sec-Octyl alcohol Butyl sulfide Isobutyl sulfide Indene Mesitylene Propylbenzene Pseudocumene Benzyl ethyl ether... 

Benzene has been amido-alkylated by reaction with ArC6H4CHClNR COR and AICI3 (R and R are various alkyl and phenyl) to ArCHPhNR COR in fair to good yields.Anisole and phenetole have been alkylated with l-chloro-2,3-epoxy-5-methylhex-5-ene and AlCls. A dissertation on apparent anomalies in the Friedel-Crafts alkylation of 2,6-dimethylphenol and its alkyl ethers has been cited. 

---