Catalysts preparation and characterization

AujC fVGC Reference Catalyst Preparation and Characterization... 

Principles and Practice of Heterogeneous Catalysis, J. M. Thomas and W. J. Thomas, Wiley-VCH 1996, 688 pp., ISBN 978-3-527-29239-4. A comprehensive textbook on classic heterogeneous catalysis which covers catalyst preparation and characterization methods. It also includes a chapter on solid-state chemistry and surface chemistry, and a chapter on process engineering. 

The experimental apparatus and the silver catalyst preparation and characterization procedure is described in detail elsewhere (10). The porous catalyst film had a superficial surface area of 2 cm2 and could adsorb approximately (2 +. 5) 10-b moles O2 as determined by oxygen chemisorption followed by titration with ethylene (10). The reactor had a volume of 30 cm3and over the range of flowrates used behaved as a well mixed reactor (10, 11). Further experimental details are given in references (10) and (11). 

Choksi, H. N., Silica Supported Binuclear Copper Catalysts Preparation and Characterization , MS thesis, Georgia Institute of Technology, (1994). 

The precursor and the calcined catalyst were characterized by various techniques such as nitrogen adsorption, mercury porosimetry, X-ray diffraction (XRD), atomic emission spectrometry by inductively coupled plasma (ICP), thermogravimetric analysis, and temperature-programmed reduction (TPR). More details about the catalyst preparation and characterization can be found in a previous work (22). 

Nguyen JV, Jones CW (2004) Effect of the synthetic method and support porosity on the structure and performance of sihca-supported CuBr/Pyridyhnethanimine atom transfer radical polymerization catalysts. 1. Catalyst preparation and characterization. J Polym Sci. Part A 42 1367... 

Acknowledaments. The authors would like to thank Dr. S. Galvagno for his contribution to catalyst preparation and characterization. Acknowledgment is made to the Donors of the Petroleum Research Fund administered by the American Chemical Sooiety for partial support of this research. Support through ARO is also gratefully acknowledged. 

Table 1 Catalyst Preparation and Characterization Basic Salt Dopants... 

Table 3 Catalyst Preparation and Characterization New Series for Pressure...

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