Calibration of differential scanning calorimeters

The heat flux and energy calibrations are usually performed using electrically generated heat or reference substances with well-established heat capacities (in the case of k ) or enthalpies of phase transition (in the case of kg). Because kd, and kg are complex and generally unknown functions of various parameters, such as the heating rate, the calibration experiment should be as similar as possible to the main experiment. Very detailed recommendations for a correct calibration of differential scanning calorimeters in terms of heat flow and energy have been published in the literature [254,258-260,269]. [Pg.181]

G. W. H. Holme, H. K. Cammenga, W. Eysel, E. Gmelin, W. Hemminger. The Temperature Calibration of Differential Scanning Calorimeters. Thermochim. Acta 1990, 160, 1-12. [Pg.260]

E. Gmelin, S. M. Sarge. Calibration of Differential Scanning Calorimeters. Pure Appl. Chem. 1995, 67, 1789-1800. [Pg.260]

ASTM E 967-92, Standard Practice for Temperature Calibration of Differential Scanning Calorimeters and Differential Thermal Analyzers, 1992. [Pg.129]

ASTM E 968-83, Standard Practice for Heat Flow Calibration of Differential Scanning Calorimeters, 1983. [Pg.129]

Price, D.M. Temperature calibration of differential scanning calorimeters. J. Therm. Anal. 1995, 45, 1285-1296. [Pg.404]

Skoglund, P. Fransson, A. Accurate temperature calibration of differential scanning calorimeters. Thermochim. Acta 1996, 276, 27-39. [Pg.404]

Sarge, S.M. Gmelin, E. Temperature, heat and heat flow rate calibration of differential scanning calorimeters. Thermochrm. Acta 2000, 347, 9-13. [Pg.3748]

E 967 (1999) Standard practice for temperature calibration of differential scanning calorimeters and differential thermal analyzers... [Pg.203]

Standard Test Method for Assessing the Thermal Stability of Chemicals by Method of Differential Thermal analysis. (Specimens weight varies from 20 to 30 mg. The reference was an empty pan. The Heat Rate used was 10 °C/min) Standard Test Method for Temperature Calibration of Differential scanning Calorimeters and Differential Thermal Analyzers... [Pg.208]

Heat flow calibration of differential scanning calorimeters ASTM E %8... [Pg.367]