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Basic Ruthenium Acetate and Mixed Valence Derivatives

BASIC RUTHENIUM ACETATE AND MIXED VALENCE DERIVATIVES [Pg.156]

Submitted by JOHN C. GOELTZ, STARLA D. GLOVER, JAMES HAUK, and CLIFFORD P. KUBIAK  [Pg.156]

A 500-mL round-bottomed flask is charged with RuCl3 3H20 (6g, 22.9 mmol), Na0Ac-3H20 (12 g, 88.2 mmol), a stir bar, 150 mL absolute ethanol, and 150 mL [Pg.156]

Department of Chemistry and Biochemistry, University of California at San Diego, San Diego, CA92093. Department of Chemistry, University of Illinois at Urbana-Champaign, Urbana, IL 61801. [Pg.156]

High-purity samples are obtained by dissolving the green powder in a minimum amount (ca. 100 mg in lOmL) of premixed 1 1 methanol/acetone, cooling to —40°C (MeCN/dry-ice bath), and collecting the precipitate from the cold solution by filtration. This recrystallization is repeated two to three times. [Pg.157]


Basic Ruthenium Acetate and Mixed Valence Derivatives 157... [Pg.157]




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Acetal derivatives

Acetals and derivatives

Acetate derivative

Mixed acetal

Mixed valence

Ruthenium acetates

Ruthenium derivatives

Ruthenium mixed-valence

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