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The Method of Debye-Scherrer and Hull

Continual variation of the angle of incidence p and the corresponding satisfaction of condition (2) may be attained in a different way. If, instead of a single crystal, a powder consisting of very many small crystals is placed in the path of an x-ray beam, it will happen in general that, because of the random orientation of the little crystals, a characteristic lattice plane will always be available for any incident angle whatsoever a multiplicity of (p values is furnished in this case by the proximity of many tiny particles. [Pg.6]

It may be added that the Laue-diagram affords the third possibility, [Pg.6]

It may be mentioned that G. D. Preston, Nature 142, 569 (1938), has recently discovered x-ray reflections of a different type, which are due to the interaction of the x-rays with the heat waVes, which travel through the lattice in all directions. [Pg.6]

The use of such layer line diagrams has frequently proved highly useful in determining complicated structures. [Pg.7]

With regard to reflection from planes which are not parallel to the axis of rotation, there is an important effect observable on irradiating a disoriented crystal powder. If, for example, the small crystals in the irradi- [Pg.7]


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