Synthesis of an acrylate-based liquid crystal polymer

Synthesis of an acrylate-based liquid crystal polymer 

Caution Carry out all procedures in a well-ventilated fume-cupboard, wear appropriate disposable gloves, a lab-coat, and safety glasses. 

Glass stirring rod Erlenmeyerflask (various sizes) Round-bottomed flask (1 L) Buchner Flask (3 L) 

Irritant highly flammable highly flammable harmful if swallowed, causes severe burns corrosive, causes burns, irritating to respiratory system 

To a two-necked round-bottomed flask (1 L) equipped with a reflux condenser, thermometer, and a magnetic stirrer bar, add 6-chlorohexanol (100 g, 0,73 mol), pyridine (58 g, 0,73 mol) and acetic anhydride (306 g, 3 mol). Heat the solution to 130°C for 1 h whilst stirring. 

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