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Solventless Microwave-assisted Reactions

The development of a solventless, microwave-assisted Suzuki reaction utilizing a readily recyclable solid catalyst offers numerous benefits. These include the straightforward recovery of both product and catalyst, conservation of energy through the use of microwave irradiation, simple commercial scale up, and low waste protocols due to the absence of solvents. Recently, Kabalka et al. reported such a procedure for the reaction between aryl iodides and arylboronic acids or vinyl boronic adds in the presence of KF-AI2O3 as a base [75a] to provide excellent yields of expected coupled products (Equation 87) [75b],... [Pg.160]

A solventless Suzuki coupling reaction has been developed using both thermal and microwave-assisted methods. A potassium fluoride-alumina mixture is utilized along with palladium powder. The KF acts as a base. ... [Pg.212]

Rebeiro, G. L., Khadilkar, B. M. Microwave assisted aromatic nucleophilic substitution reaction under solventless condition. Synth. [Pg.698]

Microwave-assisted Solventless Reactions on Solid Supports... [Pg.66]

See other pages where Solventless Microwave-assisted Reactions is mentioned: [Pg.60]    [Pg.61]    [Pg.63]    [Pg.65]    [Pg.60]    [Pg.61]    [Pg.63]    [Pg.65]    [Pg.326]    [Pg.313]    [Pg.317]    [Pg.413]    [Pg.130]    [Pg.85]    [Pg.93]    [Pg.258]    [Pg.356]    [Pg.81]    [Pg.93]    [Pg.93]    [Pg.44]   


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Assisted reactions

Microwave assisted reactions

Microwave-assisted

Solventless reactions

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