Solution X-ray scattering

Zheng, Y., Doerschuk, R C. and Johnson, J. E. (1995). Determination of three-dimensional low-resolution viral structure from solution x-ray scattering data. Biophys ]. 69,619-639. 

Solution calorimetry, 24 11-15 in bromine ttifluoride, 24 12-14 in fluorosulfuric acid, 24 11-12 in water, 24 14-15 Solution-phase reactive intermediates flow systems, 46 159-160 low temperature, 46 131-136 Solution X-ray scattering measurements, transferring, 41 409-410 Solvation, ionic, 21 211-213 Solvents... 

Kataoka, N., Kuwajima, K., Tokunaga, F., Goto, Y. (1997). Structural characterization of the molten globule of a-lactalbumin by solution X-ray scattering. Protein Science, 6, 422 130. 

Zheng, W., and Doniach, S. (2002). Protein structure prediction constrained by solution X-ray scattering data and structural homology identification. J. Mol. Biol. 316, 173-187. 

Solution X-ray scattering measurements, which make use of the power of synchrotron radiation, have now added important elements to the picture. Closed and open structures give significantly different scattering profiles (Fig. 12), especially in the medium angle range (104). These studies have shown that the opening of the N-lobe of apolactoferrin seen in the crystal structure is consistent with the solu-... 

Mould, A. P., Symonds, E.J., Buckley, P. A., Grossmann,J. G., McEwan, P. A., Barton, S. J., Askari, J. A., Craig, S. E., Bella, J., and Humphries, M.J. (2003c). Structure of an integrin-ligand complex deduced from solution x-ray scattering and site-directed mutagenesis./. Biol. Chem. 278, 39993-39999. 

Fig. 6. A plot of the characteristic peak positions (dashed line) in a solution X-ray scattering experiment (Q = 4w sin d/l, where d is half the X-ray scattering angle and 1 is 1.38 A, the wavelength of the X-rays) used to monitor the change in Na V particle size as a function of pH. The spherically averaged particle radius is shown by the solid line. The plot illustrates the highly cooperative pH dependence of the transition (Canady et al, 2001).

Picken S J, Aerts J, Visser R and Northolt M G (1990) Structure and rheology of aramid solutions X-ray scattering measurements. Macromolecules 23 3849-3854. 

Tsuruta, H. and Irving, T. (2008) Experimental approaches for solution X-ray scattering and fiber diffraction. Curr. Opin. Struct. Biol, 18, 601-608. 

The phenomenon of X-ray scattering forms the basis of techniques that serve to characterize semicrystalline synthetic polymers, to elucidate the chemical structure of biopolymers (e.g., certain proteins), and to determine size, shape and state of aggregation of macromolecules in solution. X-ray scattering is also an important tool for characterizing biopolymers such as proteins and nucleic acids in the native state. 

Seki, Y, Tomizawa, T., Hiragi, Y, and Soda, K. (2007) Global structure analysis of add-unfolded myoglobin with consideration to effects of intermolecular coulomb repulsion on solution X-ray scattering. Biochemistry,... 

Sangwoo Jin received his BE degree in 2004 from Kyungbuk National University and PhD degree in 2010 from POSTECH under the supervision of professor Ree. He has worted on the structures of functional star and block copolymers in nanoscale thin films as well as in solutions using grazing incidence and solution X-ray scattering. 

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