Reactor segmented flow tubular

Figure 8.34 Segmented flow tubular reactor (SFTR). (After Lemaitre etal., 1996, 1997)...

Doiiiiet, M., Joiigeii, N., Lemaitre, J. and Bowen, P., 2000. New morphology of calcium oxalate triliydrate precipitated in a segmented flow tubular reactor. Journal of Materials Science Letters, 19, 749-750. 

Donnet, M., Jongen, N., Lemaitre, J., Bowen, P. and Hofmann, H., 1999. Better control of nucleation and phase purity using a new segmented flow tubular reactor Model system Precipitation of calcium oxalate. In 14th International Symposium on Industrial Crystallization. Cambridge, U.K., September 12-16, Institution of Chemical Engineers, CD ROM, pp. 1-13. 

Schreiner, A., Jones, A.G., Donnet, M. and Jongen, N., 2001. Precipitation of CaC03 in the Segmented Flow Tubular Reactor (SFTR). In BIWIC-H International Workshop on Industrial Crystallization, Delft 19-20 September 2001. 

Bowen, P., Testino, A., Legagneur, V., Donnet, M., Hofmann, H., and Cobut, N., Precipitation of nanostructured ultrafine powders Process intensification using the segmented flow tubular reactor—still in search of the perfect powder, 2006 Spring National Meeting, Orlando, Florida, 2004. 

Consider the segment of tubular reactor shown in Figure 8.3. Since the fluid composition varies with longitudinal position, we must write our material balance for a reactant species over a different element of reactor (dVR). Moreover, since plug flow reactors are operated at steady state except during start-up and shut-down procedures, the relations of major interest are those in which the accumulation term is missing from equation 8.0.1. Thus... 

Layers of calcium nitrate (40 mmol T1 in water CaN03 4 H20), potassium carbonate (40 mmol 1 1 in water) and a separation layer of water are fitted into each other by means of the concentric separation mixer [53], The reaction temperature is 22 °C. The reaction solution forms droplets in a dodecane reservoir and inserted as such a segmented flow in the tubular reactor [137, 138],... 

Testing, A., Heeguijuela, J. R., Development of a continuous segmented tubular flow reactor and the scale-out concept -in search of perfect powders, Chem. Eng. Technol. 26, 3 (2003) 303-305. 

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