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Relaxation delay second order spectra

The second shortcut is to drastically reduce the digital resolution in the 2D spectrum typically the data is collected to provide 2-4 Hz per point digital resolution in the final spectrum. Typical 2 times are 0.05-0.2 s, an order of magnitude smaller than those used in ID NMR spectroscopy. The use of longer acquisition times has very little effect on data collection times. If a 1 s relaxation delay is used, increasing from 0.05 to 0.2 s results in 15% longer experiment time and provides a four-fold increase in digital resolution in fi (and a four-fold increase in the size of the data file). The same is not true in the dimension. [Pg.1208]


See other pages where Relaxation delay second order spectra is mentioned: [Pg.337]    [Pg.68]    [Pg.526]    [Pg.3397]    [Pg.104]    [Pg.511]    [Pg.312]    [Pg.587]    [Pg.144]    [Pg.126]    [Pg.706]    [Pg.110]    [Pg.226]   
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