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Pyrocatechyl phosphorotrichloridate

A soln. of GS2 in abs. ether added dropwise with stirring and ice-salt cooling to a soln. of 2 moles benzylamine in the same solvent, the precipitated benzyl-ammonium dithiocarbamate removed by filtration, dissolved in benzene, a soln. of pyrocatechyl phosphorotrichloridate in the same solvent added dropwise with stirring and ice-cooling, then refluxed 1 hr. on a water bath benzyl isothiocyanate. Y 84%. F. e., also by POGI3 instead of pyrocatechyl phosphorotrichloridate with somewhat lower yields, s. D. Martin, E. Beyer, and H. Gross, B. 98, 2425 (1965). [Pg.390]

Classification of dehydration agents s. 16, 539 Reactions with pyrocatechyl phosphorotrichloridate ... [Pg.548]

A mixture of pyrocatechyl phosphorotrichloridate and benzamide ethyl phenylcarbamate 2-acetylmesitylene... [Pg.131]

See other pages where Pyrocatechyl phosphorotrichloridate is mentioned: [Pg.146]    [Pg.435]    [Pg.92]    [Pg.565]    [Pg.131]    [Pg.144]    [Pg.146]    [Pg.435]    [Pg.92]    [Pg.565]    [Pg.131]    [Pg.144]   


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