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Pulsed field gradients implementing

Figure 2.7.2 illustrates two implementations of the diffusion-relaxation experiment using the pulsed field gradient. In the first implementation, a spin-echo... [Pg.166]

The pulsed field gradient NMR technique can be readily used for the determination of the water droplet size distribution in W/O emulsions or the oil droplet size distributions in O/W emulsions. Important advantages are the non-invasive nature, the ease of sample preparation, and the feet that pulsed field gradient NMR measures the droplet size distribution of the bulk in contrast with microscopic methods which estimate the size distribution of the surface. Both the proposed matrix method and the iterative curve fitting procedure can be successfully applied in a factory environment. The method can be implemented on a high as well as on a low resolution NMR spectrometer. [Pg.162]

BIRD-HMQC. The most difficult aspect of implementing the HMQC experiment is the suppression of signals from protons attached to C (the center-band or single quantum coherences) in favor of the protons attached to C (the satellites or double quantum coherences). The use of pulse field gradients (PFG, Section 6-6) is the most effective technique, but relatively few spectrometers are equipped with the hardware required for their generation. Fortunately, there is an effective alternative for the suppression of center bands by means of the BIRD Bilinear Rotation Decoupling) sequence, which is outlined by the vector... [Pg.189]

Parella T (1996) High quality ID spectra by implementing pulsed-field gradients as the coherence pathway selection procedure. Magnetic, Resonance in chemistry 34 329-347. [Pg.1094]


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See also in sourсe #XX -- [ Pg.186 ]

See also in sourсe #XX -- [ Pg.157 ]




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