Preparation of Vanillin from Isoeugenol

To ascertain if the oxidation of the isoeugenate of soda is complete the quantity of by drop, in which is set free at the negative polo may be measured and from it be deduced the quantity of oxygen set free at the positive pole or the test may be simply made by reference to the quantity of oxygen at the positive pole but the invention is not limited, of course, in any way to any particular test. 

The accompanying drawing illustrates diagramraatically an apparatus which may conveniently be used in carrying out our process. 

When the oxidation is judged to be complete the solution is treated with an acid which sets free the vanillin. It can be purified with bisulphide of soda and by repeated crystallization, as may be found requisite. 

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